GCMS analysis data for sample AD29466, Jan 2002

Machine-extracted title · confidence 95%

Raw GCMS analysis data and chromatogram details for sample AD29466 including surrogate recovery results.

NYC-WTC_000036603–000036613

Folder label: “GCMS X 12/6/01 A 12/12/01 - 12/13/01”

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC1301\29464.D Vial: 14 Acq On : 13 Dec 2001 10:34 pm Operator': 209 GALOS Sample : gems scan 12/6 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title 209 625/TCLP calibration table Library C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Propanol, 1-(2-methoxy-l-met Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

11.33 1.52 ug/1 554616 1,4-Dichlorobenzene-d4 11.67

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanol, 1- (2-methoxy-l-methylet 148 C7H16O3 020324-32-7 90 2 2-Butanol, 3,3' -xybis- 162 C8H18O3 054305-61-2 64 3 2-Propanol, 1 ,1 - oxybi s- 134 C6H14O3 000110-98-5 56 4 1-Propanol, 2/ (2-hydroxypropoxy)- 134 C6H14O3 000106-62-7 45 'Abundance Scan 685 (11.330 min): 29464.D (-) m/z 59.05 100.00% 59

1 5000-

39 | 45

53 . 73 103 .... M 11.00 11.20 11.40 f 11.60 ! m/z-> 20 ■ i 1 1 ■ ■ i ■ 30 -P 40 50 60 TTf 1/ 70 80 89 90 — ...................... 130 , 100 110 120 13G 140 m/z 44.95. 46.92% Abundance #9238: 2-Propanol, 1-(2-methoxy-1 -methylethoxy) 59 ...

5000 45 103 11.00 11.20 11.40 11.60 73 31 m/z 102.95 33.97% ----- ———————— TPTmT । । । J_____________ 130 ' i ' ' ■ ' i ' ' ' ' i ' ' ' 1 i ■ • ■ • i ■ m/z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #12859: 2-Butanol. 3,3'-oxybis- 59 V 1T ' 1 1 ' 11.00 11.20 11.40 11.60 5000- 31 45 m/ z 73.00 28.41% l 103 I I , i J •_______ L_______________________ :______ 134 Td11//-1/1/1"/d/EET/—11T/1/LO/B/B—EO/n—-n/-n/d/n/tI/Td/TET"TTCm—/Dd/d/n/I/B/B/nnT-n m/z-> 20 30 40 50 60 70 80 90 100 110 120 130_140 'Abundance #6087: 2-Propanol, 1,1'-oxybis- 59 11.00 11.20 11.40 11.60

NA m/z 41.05 24.59% 31 5000 45

103

miz-> ■ i ■ ■ • • i ■ > ■ ■ । i 20 30 40 T 50 60 +72.... .................... 1 ■ i ' ‘ ' i ' r ' ■ r1"1 1 1 i 1 1 1 1 i 70 80 90 100 110 120 130 140 11.00 11,20 11.40 11.60

29464.D GCMS1126.M Fri Dec 21 13:09:40 2001 Page 2

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