GCMS sample analysis report for AD29965, Jan 2002

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Laboratory analysis report for environmental sample AD29965 showing GCMS results and surrogate compound recovery rates.

NYC-WTC_000037485–000037495

Folder label: “GCMS X 12/11/01 A 12/16/01”

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\DEC1401\29965.D Vial: 49 Acq On : 16 Dec 2001 1:33 pm Operator: 209 GALOS Sample : gems scan 12/11 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Propanol, 1-(2-methoxy-l-met Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T. 11.36 0.32 ug/1 75947 1,4-Dichlorobenzene-d4 11.67 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propan , 1-(2-methoxy-1-methylet 148 C7H16O3 020324-32-7 83 2 1-Propanol, 2-(2-hydroxypropoxy)- 134 C6H14O3 000106-62-7 45 3 2-Propanol, 1- (2-methoxypropoxy )- 148 C7H1603 013429-07-7 40 4 2-Propanol, 1,1* -oxybis- 134 C6H14O3 000110-98-5 39 Abundance Scan 688 (11.357 mln): 29965.D (-) m/z 59.05 10 .00% 59

5000

miz-> Abundance • ■ i • 30 45

+115 1—2744 &o' 90 100 110 120 130 40 50 60 70 73

, 86 r_ ,

#9238: 2-Propanol, 1-(2-methoxy-1-methylethoxy) 103

।..... r NJ 'ITT TIT 1 ' r 1 I 1 ' ' 1 I ' ' IT I 1 11.00 11.20 11.40 11.60 m/z45.05 43.59%

5000 • i ■ • ■ • i • • 1 1 1 1 1 1 I 1 1 1 1 1 1 45 103 11.00 11.20 11.40 11.60 73 31 m/z 103.05 33.33% 130 ■ • — --PHH ’ ■ ■ ■ i 1 ■ m/z-> 30 40 50 60 70 80 90 100 110 120 130 Abundance #6086: 1-Propanol, 2-(2-hydroxypropoxy)- 59 .... A.... 11.00 11.20 11.40 11.60 m/z

MA 5000 41.0,0 ... 27.25% 31 45 103

— 4 1111 ■'! 75 89 1 I ‘ ‘ ‘ 1 1 1 1 ‘"I > > 1 ■ I 1 1 1 • I I • • i ■ ■ ■ ■ i ■ ■ ■ • i ■ ■ m/z-> 30 40 50 I60 70 80 90 100 110 120 130 Abundance #9233:2-Propanol, 1-(2-methoxypropoxy)- LA A 4 , M4A. . 59 11.00 11.20 11.40 11.60 m/z 73.00 27.25%

AJ 5000

31 45 ‘IT --- 3.............. 104............ 130 TOS’-T’T’OrOSTEIIITCCCITTAISTST T l IT । . m/z—> 30 40 50 60 70 80 90 100 110 120 130 11.00 11.20 11.40 11.60

29965.D GCMS1126.M Wed Jan 30 12:46:59 2002 Page 2

NYC-WTC_000037493

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NYC-WTC_000037493Source: NYC Law Department, mirrored locally

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