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GCMS analysis comments for sample AD29517 re-analysis required, Jan 2002

Machine-extracted title · confidence 95%

Laboratory comments on GCMS scan results for sample AD29517 noting low recovery and scheduling re-extraction.

NYC-WTC_000036656–000036677

Folder label: “GCMS X 12/6/01 A 12/12/01 - 12/13/01

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Scanned page image, NYC-WTC_000036667
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\JAN0302\29517.D Vial 17 Acq On 4 Jan 2002 2:10 am Operator 209 GALOS Sample gems scan Inst GC/MS 209 Mise Multiplr 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 2-Propanol, 1-(2-methoxy-l-met Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

11.27 2.31 ug/1 1159190 1,4-Dichlorobenzene-d4 11.53

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanol, 1-(2 -methoxy-l-methylet 148 C7H16O3 020324-32-7 78 2 2-Propanol, 1 ,1’-oxybis- 134 C6H14O3 000110-98-5 56 3 1-Propanol, 2-((2 -hydroxypropoxy)- 134 C6H14O3 000106-62-7 45 4 2-Propanol/ 1-(2-methoxypropoxy)- 148 C7H1603 _ 013429-07-7 40 Abundance Scan 678 (11,269 min): 29517.D (-) m/z 59.05 100.00% 59 i I 5000-

— +53 — 45

TH—— 73

85 91 , 103

........ 130.... _M 11.00 m/ z 11.20 45 05 11.40 11.60 53.11% miz—> 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #9238: 2-Propanol, 1-(2-methoxy-1-methylethoxy)- 59

5000 -

31 45 73 103 11.00 m/Z 103 05 -4V 11.20 A 11.40 11.60 30.49% . i • i ■ ■ ■ ■ i • ■ ■ ■ i > ........... i.......... 130.... ' i ■ • ■ ■ i ■ mz-> 30 40 50 60 70 80 90 100 110 820 130 140 'Abundance #6087: 2-Propanol. 1,1-oxybis- 59 V 1II-PPT 11.00 11.20 11.4C 11.60 31 5000- 45 I m/ z 73.00 26.43% 103

! ____________ !_________ ,11______ 1 1 | < | ' ' ' ' | ' ' ' > | . 1 « j B - l b | ... . J 72 89 . | | | | | . m/z-> Abundance 30___ 40 50 60 70 80 90 100 110 #6086: 1-Propanol, 2-(2-hydroxypropoxy)- 59 120 130 140 .A 11.00 11.20 11.40 11.60 m/z 41 05 25.37% 5000- 31 45 103 V -PP- 75 89 11 ■' '' । ■ ■ ■ ■ । ■ ■ ■ ■ । ■ ■ ■ ■ ।11 ■ ■ । ■''' । ■ ■ ■ ■ ।' ■ • ■ । ' m/z-> 30 40 50 60 70 80 90 100 11 120 130 140 11.00 11.20 11.40 11.60

29517.D GCMS1126.M Tue Jan 08 12:19:46 2002 Page 5

NYC-WTC_000036667

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NYC-WTC_000036667Source: NYC Law Department, mirrored locally

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