GCMS sample analysis report for AD29789, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC14O1\29782A.D Vial: 50 Acq On : 16 Dec 2001 2:32 pm Operator: 209 GALOS Sample : gems scan 12/11 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L *************************************************** * ** ** ********* * * * * Peak Number 2 2-Propanol, 1-(2-methoxy-l-met Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

11.36 0.43 ug/1 106695 1,4-Dichlorobenzene-d4 11.67

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanol, -(2-methoxy-1-methylet 148 C7H16O3 020324-32-7 83 2 2 -Propanol,1,1'-oxybis- 134 C6H14O3 000110-98-5 50 3 2-Butanol, 3,3'-oxybis- 162 C8H18O3 054305-61-2 50 4 l-Propanol, 2-(2-hydroxypropoxy)- 134 C6H14O3 ____ 000106-62-7 45 Abundance Scan 688 (11.356 min): 29782A.D (-) m/z 59.05 100.00% 59

5000

m/z-> Abundance 20 30 40 45

5 50 60 70 73

80 103

, 86...... !...... ....... 90 #9238: 2-Propanol, 1-(2-methoxy-1-methylethoxy)- 100 110 120 130 140 TT

m/z 44.95 N 11.00 11.20 11.40 11.60 50.73% IT

59

5000 "T — I" 45 103 11.00 11.20 11.40 11.60 73 31 . m/z 103.05 36.44% ..... —.... — ■ l ■ ■ ■ I mu—t ,| 130 , , , m/z-> 20 30 40 50 (60 70 80 90 100 110 120 130 140 Abundance #6087: 2-Propanol, 1,1‘-oxybis- 5’9 ' i • • • ■ i 1 1 1 1 1 1 । i 1 11.00 11.20 11.40 11.60 31 5000 45 m/z 73.00 29.01% 103

m/z-> 20 30 . -2 40 50 60 70 80 90 100 110 120 130 140 Abundance #12859: 2-Butanol, 3,3'-oxybis- ■i —TT ■ ■ 59 11.00 11.20 11.40 11.60 m/z 41.05 2__ - 6.04% 5000 31 45 103 ■ AA 134 — 4— —+ I ■ ' 1 ' i 1 ' ' r i ■ 1 ■ 1 i ■ 1 ■ ■ i ■ ’ 1drn < r i . j > > > i । i m/z—> 20 30 40 50 (60 70 80 90 100 110 120 130 140 11.00 11.20 11.40 11.60

29782A.D GCMS1126.M Wed Jan 30 11:47:49 2002 Page 2

NYC-WTC_000037424