GCMS sample analysis report for AD29965, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\DEC1401\29929.D Vial: 43 Acq On : 16 Dec 2001 7:44 am Operator: 209 GALOS Sample : gems scan 12/11 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 2-Propanol, 1-(2-methoxy-l-met Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

11.36 0.36 ug/1 80902 1,4-Dichlorobenzene-d4 11.67

Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 2-Propanol ,/1-(2-methoxy-1-methylet 148 C7H16O3 020324-32-7 83 2 2 -Butanol / 3,3 ’ -oxybis- 162 C8H18O3 054305-61-2 64 3 2-Prop. 1, 1,1’-[(1-methyl-l,2-eth 192 C9H20O4 001638-16-0 50 4 1-Prop ol, 2-(2-hydroxypropoxy)- 134 C6H14O3 000106-62-7 42 Abundance Scan 688 (11.359 min): 29929.D (-) m/z 59.05 10( .00% 59

5000

.......... ...... 45

-51——— 73

86 94 . 103

■ THtr ■ । . 11 . । ■ i ■ ■ । T . i •«>»i • N 11.00 11.20 11.40 11.60 m/z 45.05 48.75% -r-r-T-r

N miz-? 20 30 40 50 60 70 80 90 100 110 120 130'’140 Abundance. ................... a#9238: 2-Propanol, 1-(2-methoxy-1-methylethoxy)- 59

5000 ■ l 1 ■ TTmmmTgr 45 103 11.00 11.20 11.40 11.60 73 31 m/z 102.95 37.63% — TIHmm . । ■ l।_■__________ 130 > । iTT I ।T i > . . m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #12859: 2-Butanol, 3,3‘-oxybis- 59 —TnnniToT TTT t t r TTTf 11.00 11.20 11.40 11.60 5000 31 45 m/z 73.00 30.75% 103

miz—> Abundance 20 30 Li • I I l 1 ‘« > I TT 40 50 59 134 TTr TI >■>■>> j > > i > ( ri i > । i1T*—i——————Trur 60 70 80 90 100 110 #20630: 2-Propanol, 1,1‘[(1-methyl-1,2-ethanedlyl)bis(oxy) 120 130 140 TIr

m/z . NN TI——PPTTT 11.00 11.20 11.40 11.60 41.05. 26.06% 5000

miz-> 'I 11 — — 20 31

30 391 IIr 40 45

50 1 73 117 —mmHtor T_—TTTpw—u—foemproanr 60 70 80 90 103

100 110 120 130 140 M 11.00 11.20 11.40 11.60

29929.D GCMS1126.M Wed Jan 30 12:46:03 2002 Page 3

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