GCMS sample analysis report for AD29965, Jan 2002

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Library Search Compound Report Data File : C:\HPCHEM\1\DATA\DEC1401\29929.D Vial: 43 Acq On : 16 Dec 2001 7:44 am Operator: 209 GALOS Sample : gems scan 12/11 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 2-Propanol, 1-(2-methoxy-l-met Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 11.43 0.57 ug/1 125928 1,4-Dichlorobenzene-d4 11.67 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Propanol, 1-(2-methoxy-l-methylet 148 C7H16O3 020324-32-7 50 2 2-Prop. l, 1,1‘-oxybis- 134 C6H14O3 000110-98-5 50 3 Amylen Hydrate 88 C5H12O 000075-85-4 33 • 4 2-Propanol, 1,1 -[(1-methyl-1,2-eth 192 C9H2004 ______ 001638-16-0 33 Abundance Scan 696 (11.432 min): 29929.D (-) m/z 59.05 100.00% 59 5000

34 45

.I .r 51 . 73

86 94 103

, N. 11.20 11.40 11.60 11.80

M 1110110)* | i I 'I 'I l ■ ■' ■ 1’1 • i ■ 1 1 • i ■ 1 • ■ i • ' ■ • i • • । • i* m/z 45.00 50.58% mz-2 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #9238:2-Propanol, 1-(2-methoxy-1-methylethoxy)- 59

5000 103 TT TT——n.nmmBTTTT T 45 11.20 11.40 11.60 11.80 73

N. 31 m/z 103.05 34.32% - — 1I+ mTTT 130 miz-> 20 30 40 50 60 70 80 90 100 110 120 180 Abundance #6087: 2-Propanol, 1,1‘oxybis- 50 31 11.20 11.40 11.60 11.80 ' 5000 45 m/z 73.00 0.48% 103

2 miz-> Abundance 20 I | I T J I [I 111 |! 30 40 T-r-p-T 50 11»•»• । • * * • t *»»* i *»* * । * * •»। • i ■ > । * *' * 11» 60 59 80 90 100 110 120 130 70 #62940: Amylene Hydrate JM 11.20 11.40 11.60 11.80 m/z 41.05 23.33% T

73 5000 45 31

I m/z—> ' TOTrHt 1 I 1 ' 1 1 I 1 1 1 1 I TH 20 30 40 50 160 r 11 1 70 80 90 i 4 : । : i i ♦ j : it i TTTT i I T T 100 110 120 130 11.20 11.40 11.60 11.80

29929.D GCMS1126.M Wed Jan 30 12:46:06 2002 Page 4

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