GCMS sample analysis report for AD29929, Jan 2002

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Laboratory analysis report for environmental sample AD29929 showing GCMS results and surrogate compound recovery rates.

NYC-WTC_000037457–000037472

Folder label: “GCMS X 12/11/01 A 12/16/01”

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC1401\29928.D Vial: 46 Acq On : 16 Dec 2001 10:39 am Operator: 209 GALOS Sample : gems scan 12/11 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 2-Propanol, 1-(2-methoxy-l-met Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

11.42 0.88 ug/1 214823 1,4-Dichlorobenzene-d4 11.67

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Propa: 1, 1-(2-methoxy-1-methylet 148 C7H16O3 020324-32-7 72 2 1-Propa ol, 2-(2-hydroxypropoxy)- 134 C6H1403 000106-62-7 45 3 2-Propanol , 1,1’ -oxybis- 134 C6H14O3 000110-98-5 45 4 2-Bucanol, 3,3»-oxybiS-________ 162 C8H18O3 _______ 054305-61-2 39 Abundance Scan 695 (11.424 mln): 29928.D (-) m/z 59.05 100.00% 59 5000

39 -PIIP 84 45

IT I j TT ll|llll TTTT , | 73 103

{ । . M 11.00 1120 11.40 11.60 11.80 m/z 45.05 » ‘I ‘ «

51.74% mz-

NA 30 40 50 SO 70 80 90 100 110 120 130 Abundance #9238: 2-Propanol, 1-(2-methoxy-1-methylethoxy) 59

TTT*rrrrT‘111‘L

A 5000 103 T 45 11.00 11.20 11.40 11.60 11.80 73 31 m/z 103.05 38.75% TIIm Impt — ■ D ■ । ■ ■ ■ ■ । 130 ■ i • ■ • ‘ i ■ • miz-> 30 40 50 I60 70 80 90 100 110 120 130 Abundance #6086; 1-Propanol, 2-(2-hydraxypropoxy)- 59 11.00 11.20 1140 11.60 11.80 5000 m/z 7.75% 31 45 103

—————il — 75 89 i r i । . ri TTI—ornr i ( ; । i i । — TT i TTTTTTrTT m/z—> 30 40 50 60 70 80 80 100 110 120 130 Abundance #6087: 2-Propanol, 1,1'-oxybis- i T ■ ‘ I * » • I • • » * J » • 59 11.00 11.20 11.40 11.60 11.80

NA m/z 41.05 27.47% 31 5000 45 103 89 72 • • j * • ■ ■ ।' 1T 1 ■ 1 Ht | TIT II T I I I J I I I T I I j 11 11 J • I r• I I r• I I ‘ ‘II . 16n1/-//1/1t1/0n, m/z-> 30 40 50 <60 70 80 90 100 110 120 130 11.00 11.20 11.40 11.60 11.80

29928.D GCMS1126.M Wed Jan 30 12:44:42 2002 Page 4

NYC-WTC_000037467

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NYC-WTC_000037467Source: NYC Law Department, mirrored locally

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