GCMS sample analysis report for AD29929, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\DEC1401\29928.D Vial: 46 Acq On : 16 Dec 2001 10:39 am Operator: 209 GALOS Sample : gems scan 12/11 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 Ethyne, fluoro- Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

20.62 0.43 ug/1 133751 Acenaphthene-dl0 20.55

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Ethyne, fluoro- 44 C2HF 002713-09-9 3 2 Acetaldehyde 44 C2H4O 000075-07-0 3 3 Carbon dioxide 44 CO2 000124-38-9 3 4 Ethylene oxide 44 C2H40 000075-21-8 3 Abundance Scan 1697 (20.622 mln): 29928.D (-) m/z 39.95 100.00% 40

5000

45 50 55 62 78 88 94 N TTTTTTTTTg61 20.20 20.40 20.60 20.80 21.00 UTImT TTT TTggTg m/z 43.95 59.08% miz-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 Abundance #35: Ethyne, fluoro- 444

5000 T T T l 1 ' ‘ ' I ‘ ■ 20.20 20.40 20.60 20.80 21.00 25 31 m/z 35.85 1.75%

miz- 5 +13,19 mrm TIUTTIITT Uouu—gpmpmpEODaUpt 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 Abundance #36: Acetaldehyde 29 44 20.20 20.40 20.60 20.80 21.00 5000 m/z 77.95 1.29%

24,. i ■ ■i••" i miz—> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 Abundance #34: Carbon dioxide I ' ‘ ' 1 I T 44 20.20 20.40 20.60 20.80 21.00 m/z 44.75 1.21% 5000

16 22 TITTTTg 11 < 111 ■> 11111111 T’’EI’T__TOITTITI"EITI I 1 ' 1 4 ! ■ ■ 1" i • ■ 1 ■ i i" ■ ■ i 1 ‘ 1 1 1 miz—> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 20.20 20.40 20.60 20.80 21.00

29928.D GCMS1126.M Wed Jan 30 12:44:46 2002 Page 5

NYC-WTC_000037468