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GCMS sample analysis report for AD29929, Jan 2002

Machine-extracted title · confidence 100%

Laboratory analysis report for environmental sample AD29929 showing GCMS results and surrogate compound recovery rates.

NYC-WTC_000037457–000037472

Folder label: “GCMS X 12/11/01 A 12/16/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\DEC1401\29928.D Vial: 46 Acq On : 16 Dec 2001 10:39 am Operator: 209 GALOS Sample : gems scan 12/11 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 6 Anthracene-dlO- Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T. 25.12 0.31 ug/1 92212 Phenanthrene-dl0 24.97

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Anthrac 2 Phenant rene-d19 / ne-d10,4 188 C14D10 188 C14D10 001719-06-8 28 001517-22-2 25 3. 4-Methyl-2- (3-fluorophenyl)pyrimidi 188 C11H9FN2 076128-66-0 9 4 4-Me/hyl-2-(4-fluorophenyl)pyrimidi 188 C11H9FN21 076128-67-1 9 Abundance Scan 2187 (25.121 min): 29928.D (-) m/z 188.10 100.00% 188

5000 80 94 54 132 160 I I I ll f ) I l t 11gb I I I I » I I I } 24.80 25.00 25.20 25.40 ul +1 , 1 J, L -1 1 mt ll m mlz-> ’ 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 m/z 94.00 34.21% Abundance #19957: Anthracene-d10- 188

5000 T 1 T I 24.80 25.00 25.20 25.40 m/z 80.05 29.66% 66 80 9 TH TIIrr 160 mHHm "T T‘ T 1 “ ’' I miz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19958: Phenanthrene-d10 188

24.80 25.00 25.20 25.40 5000 m/z 160.05 20.37% 80 94 160 • 66 • i • ‘ “i “ “ i “ *' i" ‘‘It — P > T m mm — r miz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19859: 4-Methyl-2-(3-fluorophenyl)pyrimidine 1 1 1 11 188 24.80 25.00 25.20 25.40 m/z85.8516.26% 5000

miz—> 67 75 i 14 1 i i | i ! t । I i i I 11 ...... i j j 11 ii ...... 94............ i j rm ji 121

j r* vj rnr TI’’’II T 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 146 161 | 173 | (r. ।।। .11. ।.'i - 0 • ‘ l '" • ' I ‘ ■ I • ‘ 24.80 25.00 25.20 25.40 ' I T

29928.D GCMS1126.M Wed Jan 30 12:44:50 2002 Page 6

NYC-WTC_000037469

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NYC-WTC_000037469Source: NYC Law Department, mirrored locally

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