GCMS blank analysis results for sample AD31586, January 2002

Machine-extracted title · confidence 100%

Laboratory report of a GCMS blank analysis for sample AD31586 listing chemical compounds with results below detection limits.

NYC-WTC_000049684–000049692

Folder label: “GCMS X 1/2/02 A 1/3 - 1/4/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C: \HPCHEM\ 1 \DATA\JANO 3 02 \ LBB. D Vial: 31 Acq On 4 Jan 2002 3:45 pm Operator: 209 GALOS Sample gems scan 1/2 a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Anthracene-dlO- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

24.96 0.24 ug/1 64084 Phenanthrene-dl0 24.81

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-dlO- 188 C14D10 001719-06-8 83 2 Phenan rene-dlO 188 C14D10 001517-22-2 50 3 4-Meth; 1-2-(4-fluorophenyl)pyrimidi 188 C11H9FN2 076128-67-1 9 4 Cyclohexanone, phenylhydrazone 188 C12H16N2______ 000946-82-7 9 Abundance Scan 2169 (24.956 min): LBB.D (-) m/z 188.10 100.00% 1(18

5000

.. 52 66 80 94 158 i n PI 1.11 i 11 r| i .11 Fit+j 11 i i j i > i i | i 11 i | ri i q i ni|-ri ri 11 i tl'l n i. ।. .. . |’ m 24.60 24.80 25.00 25.20 m/z 94.00 15.88% m/z~> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19957: Anthracene-d 10- 158

................................... ............. 5000 24*60 24.80 25.00 25.20....... 94 m/z 184.05 11.91% 66 80 — rr|rn T-j-r 11 rt. H I | ri i q i n , rU an ------ ‘•‘1’11’1/14468 m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19058: Phenanthrene-dW 188 1 ri 1-1 f i g 24.60 24.80 25.00 25.20 5000 m/z 80.05 11.41% 160 66 80 94 TIPWTCTITTLLTTPWTITTPPIWPPIUTT PPmmpem mfe-> 30 40 50 60 70 80 90 100 110 120 130 140 150 .160 170 180 190 Abundance #19860:4-Methyl-2-(4-fluorophenyi)pyrimidine 188 24.60 24.80 25.00 25.20 ‘ ‘ 1 ‘ 121 m/z 65.95 8.03% 5000 173 57 7 75 84 102; | 146 ..।.... ।. 11. i.).... 111,11.. 11..■ 1 | > I I > /I . i I । ■ M > | 1 I l'i । > i . . । i . i i । . Tgur1 ITUT l . HT i । । ( . m/z—> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 24.60 24.80 25.00 25.20

LBB.D GCMS1126.M Fri Feb 01 11:33:12 2002 Page 2 NYC-WTC_000049691

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