GCMS analysis results for sample AD31641, February 2002

Machine-extracted title · confidence 100%

GCMS analysis report for sample AD31641 conducted on February 11, 2002.

NYC-WTC_000049745–000049761

Folder label: “GCMS X 1/2/02 A 1/3 - 1/4/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\1\DATA\JAN0302\31641.D Vial: 39 Acq On 4 Jan 2002 11:32 pm Operator: 209 GALOS Sample gems scan 1/2a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 Anthracene-dlO- Concentration Rank 9

R.T. EstConc Area Relative to ISTD R.T.

24.95 0.24 ug/1 61496 Phenanthrene-dl0 24.81

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Anthracene- dlO- 188 C14D10 001719-06-8 86 2 Naphthalene, 1, 7-dimethoxy- 188 C12H1202 005309-18-2 53 3 Naphthalene, 1,5- dimethoxy- 188 C12H1202 010075-63-5 42 4 2-Quin inecarboxaldehyde, 8-hydrox 188 C10H8N2O2 005603-22-5 42 Abundance Scan 2169 (24.954 mln): 31641 .D (-) m/z 188.10 100.00% 1118

5000

94 . 1...... . j 18 | *—T V T I • • » '4 J • > 4 • I • 42 54 66 80 158 . 207 H 24.60 24.80 25.00 25.20 ■ । > 111141 ■, fl 111 j ■ 1111 r 11,11 ■ 11}41.. t.... mqmmm" I m/z 9 .95 18.56% miz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 Abundance #19957: Anthracene-d10- 118

■ । /V ............................. । i । , i , । । p ri 11 5000 24.60 24.80 25.00 25.20 m/z 18 .10 14.39% >।>iii{Hit ।iiii।>iI>। 66 80 94 • i i (> > i I । ll i ■ ) I • •4 ‘ I ml 160 'I-'m11 miz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 Abundance #19813: Naphthalene, 1.7-dimethoxy- 173 188 T T 24.60 24.80 25.00 25.20 5000 m/z 8 .05 9.71% 102 115 145 i 51 63 75 130 158 TMWWWngum TCC*u—umpmnma—Bm—m—a—mnaonn mphp TWuuuar miz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 Abundance #19912: Naphthalene, 1,5-dimethoxy- TI8 । . i । . . . . । . . r। । . 188 24.60 24.80 25.00 25.20 173 m/z 6 .95 9.00% 115 5000

143 102 ....... 51 63 76........ ............... 127 I j 11111 > I IT] n-TT| 1'1 u p i-l 111111 | I I > 111 n 1111'111 n I'l | m i । Ur mmpmm . । . । . /1 rvi i । r.. r । । . i. t . miz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 24.60 24.80 25.00 25.20

31641.D GCMS1126.M Fri Feb 01 11:16:51 2002 Page 4 NYC-WTC_000049755

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NYC-WTC_000049755Source: NYC Law Department, mirrored locally

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GCMS analysis log for sample AD30696, Jan 2002 · Box DEP Box 16

NYC-WTC_000018123

Automated laboratory log recording GCMS analysis of sample AD30696 including detection of unknown compounds and surrogates.

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