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GCMS analysis results for sample AD31641, February 2002

Machine-extracted title · confidence 100%

GCMS analysis report for sample AD31641 conducted on February 11, 2002.

NYC-WTC_000049745–000049761

Folder label: “GCMS X 1/2/02 A 1/3 - 1/4/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\JANO3O2\31641.D Vial: 39 Acq On 4 Jan 2002 11:32 pm Operator: 209 GALOS Sample gems scan l/2a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C: \DATABASE\NBS7 5K. L ********************************************************************* Peak Number 3 Benzoic acid, 2,5-bis(trimethy Concentration Rank 8 R.T. EstConc Area Relative to ISTD R.T.

14.17 0.28 ug/1 74573 Naphthalene-d8 15.12

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Benzoic acid, 2,5-bis(trimethylsilo 370 C16H30O4Si3 003618-20-0 47 2 Benzoic acid,2,6-bis (trimethylsil 370 C16H3004Si3 003782-85-2 33 3 Benzenee thanamine, N-[(pentafluorop 475 C21H26F5NO2Si2 055429-85-1 32 4 Benzeneethanamine, N- (pentafluorop 563 C24H34F5NO3Si3 055429-13-5 25 Abundance Scan 994 (14.167 mln): 31641 .D (-) m/z 73.00 100.00% 73

5000 267 .r - 355 45 13.80 14.00 14.20 14.40 mhmp 11103 133 154 177 193 _ 223 251 | 323339 | p»> 1111 ?111 > i*i p i*i r'l > ir11 r*i,।11 , , ।,T.. j.», TIWWITTTDTTTT t m/z 267.00 33.19% mlz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #73978: Benzoic acid, 2,5-bis(trimethylsiloxy)-, trimethyls 73 355 1* 5000 13.80 14.00 14.20 14.40 45 m/z 355.0 22.88% i।i।I 147 179 207223 , 267282 370 Tm-rr TT] miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #51296: Benzoic acid, 2.6-bis[(trimethylsilyl)oxy]- trimet 713 355 ...................... ( .......................... » j I }*}** II I I I I I I 11 I I I I I 13.80 14.00 14.20 14.40 5000 m/z 267.90 8.94% 147 267 47 208 249 1 283 . i 370 TT P* “ I • ’ ‘T 1“ " 111111 "“I ■ ■ ■ ■ i ■1"i' ■■•i4■•■i••••i■ n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #74573: Benzeneethanamine, N-{(pentafluorophenyl)methylene] TI.n T T Tr 73 13.80 14.00 14.20 14.40 m/z 356.0 8.32% 5000 267 44 I................... 151 179 209 250 1 TIuugmTTp >1*7 n FTr u ! I ri 11111! > 11T|11 ■ ■■! ■ I n-nT ■*,. 11 > 11. । >. ■. [ • i 1 • ' • i 1 • • • • ' ■ ■ l 1 ■ • ■ i • rn/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 13.80 14.00 14.20 14.40

31641.D GCMS1126.M Fri Feb 01 11:16:47 2002 Page 3 NYC-WTC_000049754

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NYC-WTC_000049754Source: NYC Law Department, mirrored locally

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