GCMS analysis results for sample AD31641, February 2002

Machine-extracted title · confidence 100%

GCMS analysis report for sample AD31641 conducted on February 11, 2002.

NYC-WTC_000049745–000049761

Folder label: “GCMS X 1/2/02 A 1/3 - 1/4/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\1\DATA\JAN0302\31641.D Vial: 39 Acq On 4 Jan 2002 11:32 pm Operator: 209 GALOS Sample gems scan l/2a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Propanone, 1,1,1-trichloro- Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

7.60 1.32 ug/1 279477 1,4-Dichlorobenzene-d4 11.52

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanone, 1, -trichloro- 160 C3H3C130 000918-00-3 38 2 2-Pentanone, •4- roxy- 4 -methyl - 116 C6H12O2 000123-42-2 17 3 1-Propanamine 59 C3H9N 000107-10-8 9 4 2-Propanone, :1,I-dichloro- 126 C3H4C12O 000513-88-2 9 Abundance / Scan 279 (7.603 min): 31641 .D (-) m/z .95 100.00% 43

5000

59 TIT ■' ■ i • • • • i • • • • i ■ • ■ ■ i • • 7.20 7.40 7.60 7.80 8.00 J ’i 1111 ■ ii ।83I'l'i 111 ■ irr । n ■ ■t’rgertfr 125 207101 । ■ । T"Tuu"aun“B—B"B—Um—BB"8’83n7 m/z 59.Q0 18.58%

. AJ miz-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance #12247:2-Propanone, 1,1,1-trichloro- 43

5000 MmA rn 11 i ।। । । i r pTT? A 7.20 7.40 7.60 7.80 8.00 15 m/z 100.95 8.18% 85 97 125 ..!. . , . | Tmp . I > l'l 111' I.... ।11.,. ।,... j.... ।. <.. (. 11.. ।।,... । ■... (;... ।> miz-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance #64274:2-Pentanone, 4-hydroxy-4-methyl- 43 ... ......... A./ yA ■ “I1 >' 7.20 7.40 7.60 7.80 8.00 5000 m/z 58.05 7.59% 59

mfe-> Abundance namaspauoag—un 27 101 83 ImOn)pOn"an9p—mn—p=mnma*aB—p—BBVp——maa P TTTNI 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 30 #62341:1-Propanamine . A.. 7.20 m/z 7.40 4?.05 7.60 7.80 8.00 4.89% 5000-

59 42 | nppt Tm rm ।|» smn i j n »»। i »•» ।» i»» । i i » » 111 « »। « »» k ।» 11 11 » i H j. U 1Ti Pi n MPrfr m/z—> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 7.20 7.40 7.60 7.80 8.00

31641.D GCMS1126.M Fri Feb 01 11:16:42 2002 Page 2 NYC-WTC_000049753

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NYC-WTC_000049753Source: NYC Law Department, mirrored locally

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GCMS analysis log for sample AD30696, Jan 2002 · Box DEP Box 16

NYC-WTC_000018123

Automated laboratory log recording GCMS analysis of sample AD30696 including detection of unknown compounds and surrogates.

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