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GCMS analysis results for sample AD31640, February 2002

Machine-extracted title · confidence 100%

GCMS analysis report for sample AD31640 conducted on February 11, 2002.

NYC-WTC_000049762–000049773

Folder label: “GCMS X 1/2/02 A 1/3 - 1/4/02

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Scanned page image, NYC-WTC_000049771
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C: \HPCHEM\1\DATA\ JAN03 02\31640 . D Vial: 36 Acq On 4 Jan 2002 8:38 pm Operator: 209 GALOS Sample gems scan l/2a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

7.60 1.32 ug/1 246548 1,4-Dichlorobenzene-d4 11.52

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Pentanone, 4-hydroxy-4-methyl- 116 C6H1202 000123-42-2 42 2 2-Propanone, 1,1,1-trichloro- 160 C3H3C130 000918-00-3 16 3 2-Tridecanone 198 C13H260 000593-08-8 9 4 2-Propanone, 1,1-dichloro- 126 C3H4C120 000513-88-2 9 Abundance Scan 279 (7.604 mln): 31640.D (-) m/z 4 .95 100.00% 43

5000 59 10200 rT"r‘s "I -1" I 101 7.20 7.40 7.60 7.80 8.00 ‘‘‘‘I . .1 69 83 .J 125 ToTHmHtmpmm*mppmmmmmpmmmmmpp m/z 59.05 29.82% mlz-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200 Abundance #64274:2-Pentanone, 4-hydroxy-4-methyl- 43

5000 .111844**** TTTrpr 59 7.20 7.40 7.60 7.80 8.00 m/z 101. 10.83% 27 . 1 83 191 I l T—uepop*ammmnmnumpmep—n——nm—n1pDgppu rrp-TTTp-rrrpT m/z-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200 Abundance #12247:2-Propanone, 1,1,1-trichloro- 43 i For —4- • !»••• [* i‘ | 7.20 7.40 7.60 7.80 8.00

J. 5000 m/z 58. 8.42% 15 85 97 125 TI—m9mnma—enn"—unrTppmmmmmmpmmmmp iz-> 10 20 30 40 50 60 70 80 90 100110 120130140150 160170180190200 Abundance #69644:2-Tridecanone ■' » ■ । • 43 58 7.20 7.40 7.60 7.80 8.00 m/z 42.00 5.27% 5000 71 27 85 96 110 140 198 11 n |'n n * p ITTTi 111111111111 mrrmn “ ।.Hij >.it|n <»।* < h।< 11 (t... i p i.. t... i ।... -IPPmpTpffftr m/z—> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200 7.20 7.40 7.60 7.80 8.00

31640.D GCMS1126.M Fri Feb 01 11:14:29 2002 Page 3 NYC-WTC_000049771

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NYC-WTC_000049771Source: NYC Law Department, mirrored locally

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