GCMS analysis results for sample AD31640, February 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\JAN0302\31640.D Vial: 36 Acq On : 4 Jan 2002 8:38 pm Operator: 209 GALOS Sample : gems scan l/2a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Silane, tetramethyl- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

7.47 4.74 ug/1 885153 1,4-Dichlorobenzene-d4 11.52

Hit# of 5 • Tentative ID MW MolForm CAS# Qual 1 Silane, tetramethyl- 88 C4H12Si 000075-76-3 9 2 N-Ethyl formamide 73 C3H7NO 000627-45-2 9 3 Pentane, 3-methoxy- 102 C6H140 036839-67-5 9 4 1-Butanamine, 3-methyl - 87 C5H13N 000107-85-7 7 Abundance Scan 264 (7.466 min): 31640.D (-) m/z 73.00 100.00%

1 73

5000 43 "’I ।»> TT11 ’ 7.20 7.40 7.60 " 7.80 38 |, —TPmT ' ‘ • i ■ • ■ 1 i ' ‘ | 50 55. 60 67, । , 87 103 0- —ITTH • i ■ i ■ • m/z 43.0.0 32.17% /z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #62932: Silane, tetramethyl- 73

5000 1 ■ ■ i1 • ■ 11 7.20 7.40 ' 7.60 7.80 45 m/z 45.0 5 11.14% 15 i 53 59 । 88 SI-—-n———B/I9—BOTTTTTTTTPI ' i ■ • 1 ‘ i • ■ • ■ i • ■ ■ ■ i ‘ ' miz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #292: N-Ethylformamide 30 73 -•T-r-. ■ T TD Tsui 14Em T Ti 7.20 7.40 7.60 7.80 5000 m/z 41.0,5 10.96% 44 58

15 *— । m । > i • > । * . > l , < । । > । । । । i । , i । i । t ^ > * । < > > < । > > miz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #1793: Pentane, 3-methoxy- =T"epvvTfToui 73 7.20 7.40 7.60 7.80 m/z 71.0,0 6.95% 5000 45

27 33 39, 55 • • i • • ■ • i • • • • i • • • ‘i ■ > • • i ' d’si .... pi । ■ i ■ ■ ' ■ i ■ ■ ■ • i ■ ■ ■ • i • miz-> 10 20 30 40 50 60 70 80 90 100 110 7.20 7.40 7.60/7.80

31640.D GCMS1126.M Fri Feb 01 11:14:25 2002 Page 2 NYC-WTC_000049770