GCMS analysis results for sample AD31640, February 2002

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Library Search Compound Report

Data File C:\HPCHEM\l\DATA\JAN0302\31640.D Vial: 36 Acq On 4 Jan 2002 8:38 pm Operator: 209 GALOS Sample gems scan l/2a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Toluene Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

5.75 0.38 ug/1 70746 1,4-Dichlorobenzene-d4 11.52

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Toluene 92 C7H8 000108-88-3 90 22,5-Norbornadi ene 92 C7H8 000121-46-0 59 3 1,3,5-Cycloheptatriene 92 C7H8 000544-25-2 47 4 1,5-Heptadien-3-yne 92 C7H8 003511-27-1 45 Abundance Scan 77 (5.749 mln): 31640.D (-) SI " "7 100.00% 5000 TT-j-n-r-r-j-r-r TJBnnR—mgv 39 45 51 61165 77 86, 5.40 5.60 5.80 6.00 111 p 111 p 111 p 11 ip 111 p 111111111 h n p i r II111111 p 111 p i ii p 11111 ■ 1I1 - i' i1"11 “ m/z 92.00 57.18% miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 Abundance #83029: Toluene S1

5000 —PPPTTTP 5.40 5.60 5.80 6.00 m/z 65.05 12.21% 45 51 61 65 I ■ 1111 i ■ । ■ p ■ ■ 11 I ■ । ■ | I in I 11 ■ ■ [ rH I I ■ ■ I i|-rri ■ p ■ ■ ■ p ■ i ■ pi 11 | hpoampo miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 Abundance #63032: 2,5-Norbornadiene 91 1 1 1 ' 1 1 1 1 1 1 .[M > | M I ! 5.40 5.60 5.80 6.00 5000 66 m/z 39.00 11.10%

....... 27........... 41 51 62 J...................... .. “ I “ “ I 1 ' “ I ' • ' 1 I ‘ " 1 I ITTT > 11 > | 11 i 11 l l > > 11 । i 11. 1. । . i. . t.. .. । . l .. j i l. 1) J

AooWuabw •• i “ ■11 “ m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 Abundance #63035:1,3,5-Cycloheptatriene 91 5.40 5.60 5.80 6.00’’’ m/z 62.9.5 9.75% 5000

65 27 37 46 51 11 p 111 p 111 p 11 rp 111 [l I ri 1i11I ri i1ii111I11I 61,| 111 TOTTI -rrp-rrrp-r 5.40 5.60 .M, .....' 5.80 6.00 m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100

31640.D GCMS1126.M Fri Feb 01 11:14:20 2002 Page 1 NYC-WTC_000049769