GCMS analysis results for sample AE08839, April 26, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\APR2302\8840.D Vial: 9 Acq On : 23 Apr 2002 10:14 pm Operator: Sample : gc/ms scan 4/15 fb Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Toluene Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T.

6.36 0.68 ug/1 101382 1,4-Dichlorobenzene-d4 12.21

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Toluene 92 C7H8 000108-88-3 91 2 2,5 -Norbornadiene 92 C7H8 000121-46-0 64 3 Cyclobutene, 2-propenylidene- 92 C7H8 052097-85-5 59 4 Tetracyclo[3.2.0.02,7.04,6]heptane 92 C7H8 000278-06-8 45 Abundance Scan 144 (6.365 min): 8840.D (-) m/z 91.00 100.00% 91

5000 ....... / 39 6.00 6.20 6.40 6.60 6.80 | 45 0 +TTIWWTITTTTTTTHTTTT TImg 51 .... 61.65 .... 74....... 86 —Tmmu m/z 92.00 55.73% miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 Abundance #63029: Toluene 91

- 5000 600 6.20 6.40 6.60 16.80 m/z 39.05 11.59% 45 51 65 i ** ** । ** • * । ■ ■ * ■ i —ppt lz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 Abundance #63032:2,5-Norbornadiene 91 * i * ■ ■ * i * 6.00 6.20 -4 6.40 AA-A- 6.60 6.80 5000 66 m/z 64.95 9.86%

.. 27... 41.. 51 11162a - m ।' !'■ ■' l" ■ ■ i ■ ■' ‘ i ‘‘ i ■ • ■ • i ■ ■ ■' I''11111'' 11"' I'

miz-> 20253035404550556065 70 7580859095 100 Abundance #964: Cyclobutene, 2-propenylidene- 91 6.00 6.20 6.40 6.60 6.80 m/z 51.00 6.65%

5000

65

“ i■■■■i■" ■i■■ “ i■■ ■' i ■11 ■ i ■ 51 61, rmrmm 1 |77I I I................... ■ ■■11■■■i ■ ■" ।" i1 ............... I|II!I|>! I| 1' i" " i ■ ■ MMM miz—> 20 25 30 35 40 45 50556065 70 75 808590 95 100 6.00 6.20 6.40' ' 6.60 6.80

8840.D GCMS0412.M Wed Apr 24 08:37:33 2002 Page 1

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