GCMS analysis results for sample AE08686, April 26, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\APR2202\8686.D Vial: 8 Acq On : 22 Apr 2002 4:01 pm Operator: Sample : gc/ms scan 4/11 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Toluene Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

6.36 0.44 ug/1 51794 1,4-Dichlorobenzene-d4 12.21

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Toluene 92 C7H8 000108-88-3 2 Tetracyclo[3.2.0.02,7.04,6]heptane 92 C7H8 000278-06-8 64 3 2,5-Norbornadiene 92 C7H8 000121-46-0 45 4 1,3,5-Cycloheptatriene 92 C7H8 000544-25-2 37 Abundance Scan 144 (6.365 min): 8686.D (-) m/z 91.00 100.00% 91

5000

' I ' ‘ ‘ ' I ' ‘ ‘ ' I ‘ ‘ ‘ I ‘

39 45 51 65 6.00 6.20 6.40 6.60 6.80 “ i■ I'' " I --H i"11177 86 '111111111"111 —ppe m/ z 92.00 60.67% mz—> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 Abundance #63029: Toluene 91

5000 6.00 6.20 6.40 6.60 6.80 m/z 64.95 10.94% 45 51 ■ ■ i “' • i “ “ i" " i ■" ■ i “ “ 11 ■ ■■ H' 61.65 i ■ ■ “ i •1'11 • MIIBBaopopuu +ppo miz-> 20253035404550556065 70 75 80 85 90 95 100 Abundance #963: Tetracyclo[3.2.0.02,7.04,6]heptane 91 .............. TIt6/81 1**1’’’1*’**1* A............ 6.00 6.20 6.40 6.60 6.80 5000 m/z 39.05 9.04% 66

27 38 51 ■ 1111111111 mmmtt 111" “ 111 " i ■1111'" ■ i ■ ■ ■ • i "1 ■ i •' “ i1' ■ ‘ i ■"' i"11 miz-> Abundance 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 #63032:2,5-Norbomadiene 91 ........ MAA 112.4 1-1 I ‘ ‘ ’ * 1 1 * ‘ 1 I ‘ 6.006.20 6.40 6.60 6.80 ’

m/z 62.95 5.64% 5000 66

TT[-a)—27 41 51 —u—mnOnmmHg —2-m+H fmmpo n/z—> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 6.00 6.20 6.40 6.60 6.80

NYC-WTC_000048930