GCMS sample AE08755 results, April 26, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\APR2202\8755.D Vial: 11 Acq On : 22 Apr 2002 6:58 pm Operator: Sample : gc/ms scan 4/11 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 1, Toluene Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

6.37 0.78 ug/1 104025 1,4-Dichlorobenzene-d4 12.21

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Toluene 92 C7H8 000108-88-3(91 2 2,5-Norbornadiene 92 C7H8 000121-46-0 50 3 1,3,5-Cycloheptatriene 92 C7H8 000544-25-2 47 4 Tetracyclo[3.2.0.02,7.04,6]heptane 92 C7H8 000278-06-8 47 Abundance Scan 144 (6.369 min): 8755.D (-) m/z 91.00 100.00% 91

5000 1 7 20 — 65 6.00 6.20 6.40 6.60 6.80 745 51 61 | 77 86 . m/z 92.00 61.83% I" " I ‘ “11 | ! I I I | t I , I | I I > 1 | fi I | I I 1 > | t I I 1 | ■. ... | . ..Ip... | .... | I . . I | hmmiyui miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 Abundance #63030: Toluene 91

5000 ' i ■ ■ ■ ■ i ■ 1 ■ ■ i ■ 1 ' ■ i ■ ■ ■ । • 6.00 6.20 6.40 6.60 6.80 m/z 64.95 11.41% 65 45 51 miz—> I “ “ I ‘ ‘1 ‘ I ‘ ‘ ‘ I “ " I —P 20 25 30 35 40 45 50 55 60 K 70 75 80 85 90 95 100 $144 TTTTH 1 ‘ i ““i“

Abundance #63032:2,5-Norbornadiene SI . s ... 6.00 6.20' ' 6.40 6.60 6.80 5000 66 m/z 39.05 8.31%

27 41 51 I11| - mmmmmmH Hpmp miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 Abundance #63035:1,3,5-Cycloheptatriene n w AA 91 6.00 6.20 6.40 6.60 6.80 m/z 62.95 5.99% 5000

65 27 37 " I “ “ 111'11'" 11" “ I " “ I' ‘ 46 51 ।<■■•। 61 " i111111 ■ ■ ■ I'“11'■'‘I““I“111 ■ ■ i ■11' i “ M mfz~> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 6.00 6.20 6.40 6.60 6.80

NYC-WTC_000048960