GCMS sample analysis report for AD29965, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\DEC1401\29929.D Vial: 43 Acq On : 16 Dec 2001 7:44 am Operator: 209 GALOS Sample : gems scan 12/11 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Silane, tetramethyl- Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 7.59 3.66 ug/1 813233 1,4-Dichlorobenzene-d4 11.67 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 SilaneJ tetramethyl- 88 C4H12Si 000075-76-3 50 2 Pentane, 3-methoxy- 102 C6H140 036839-67-5 25 3 N-Ethylformamide 73 C3H7NO 000627-45-2 9 4 Butane, 2 -methoxy-2-methyl - 102 C6H140 ______ 000994-05-8 9 Abundance 1 Scan 278 (7.595 min): 29929.D (-) m/z 73.00 100.00% 73

5000 43 • i • ■ • ■ i ■ ■ i • 1 1 4 i • ■ 7.20 7.40 7.60 7.80 8.00 101/ 1 67, 381, , TT48T Tr55., 11t , T T "T TT87J 'j k T T T J 103 1418 TT m/z Td1r ■ • 11 T—TTTtf T I TT 'l miz-? 10 20 30 40 50 60 70 80 90 100 110 Abundance ' #62932: Silane, tetramethyl- 73

5000 •n-rmi IT 7.20 7.40 7.60 7.80 8.00 45 m/z 44.95 11.20% 15 , J 53 59 __ _______ 88 —4 — 4 TIIITITI 11/*n/—n0nDtn[1nd/1.n mz—> 10 20 30 40 50 60 70 80 90 100 110 Abundance #1793: Pentane, 3-methoxy- 73 TT71 r TT Buruengr TTa—r 7.20 7.40 7.60 7.80 8.00 5000 m/z 41.0,5 10.88% 45 I i 27 33 39 55 - miz-? ■ ■ i 4 ■ • 4 f 4 10 20 1′30’ ‘ 40 50 60 70 80 90 100 110 Abundance ............... . #292: N-Ethylformamide FTPm—n TTYTPrr 30 7.20 7.40 7.60 7.80 8.00 73 m/z 71.00 6.79% 5000 44 58

15 —II • 4 1 1 t • I’ । । i 11—uu—u—um—etTT?rrtnr m/z-> 10 20 30 40 50 60 70 80 90 100 110 7.20 7.40 7.60 7.80 8.00

29929.D GCMS1126.M Wed Jan 30 12:45:55 2002 Page 1

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