GCMS sample analysis report for AD29965, Jan 2002

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Library Search Compound Report Data File : C:\HPCHEM\1\DATA\DEC1401\29929.D Vial: 43 Acq On : 16 Dec 2001 7:44 am Operator: 209 GALOS Sample : gems scan 12/11 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Propanone, 1,1,1-trichloro- Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 7.73 0.82 ug/1 181770 1,4-Dichlorobenzene-d4 11.67 Hit# of 5 Tentative ID MW MolForm CAS# Qual l 2-Propanone 1,1,1-trichloro- 160 C3H3C130 000918-00-3 38 2 2-Propan e. 1,1-dichloro- 126 C3H4C120 000513-88-2 23 3 Cyclopentanol, 2-methyl-, acetate, 142 C8H14O2 040991-94-4 9 4 Ethanol, 2,2,2 - trichloro- 148 C2H3C130 000115-20-8 9 Abundance Scan 293 (7.732 mln): 29929.D (-) m/z 4 .00 100.00% 4)3

5000 — Trre TT 49 56 63 70 82 7.40 7.60 7.80 8.00 1 • 1 ‘ 37 97,103 • i ■ ‘1 ■ i ■ • THT 1 -Im’r TOPIrTTTprotptt 117.125 m/z 46.90 7.81% miz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #12247: 2-Propanone, 1,1,1-trichloro- 43 -WWvwWAww 5000 ’-1/11*1111/1/1/6/1/111/7888 7.40 7.60 7.80 8.00 15 rn/z 124.85 7.18% 35 49 85 97 117 125 • ■ i1 1 I 1 ' ' 1 1 1 *'• 1 I 1 HOuumgTtnu—uHpTmmgr miz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #4368: 2-Propanone, 1,1-dichloro- 43 . T 7.40 7.60 7.80 8.00 5000 m/z 81.95 6.89% 15 07 | 7 37 49 63 76 83 93 1uun——uu—pmpmPPITTTT m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #7952: Cyclopentanol, 2-methyl-, acetate, trans- T T 4)3 7.40 7.60 7.80 8.00 m/z 126.90 6.26% 5000 82 67 55 I 1 100 TBIBtssTTTrTuyr 11111 44 — 1 • __• iI ----- 1 ' ‘ i1 ■ ■ ■ । • 111 > । > 1111 miz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 7.40 7.60 7.80 8.00

29929.D GCMS1126.M Wed Jan 30 12:45:59 2002 Page 2

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