GCMS analysis results for sample AD29783, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC1401\29783.D Vial: 6. Acq On 15 Dec 2001 7:25 am Operator: 209 GALOS Sample : gems scan 12/10 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ******************************************************************* ** Peak Number 5 2-Propanone, 1,1,1-trichloro- Concentration Rank 11

R.T. EstConc Area Relative to ISTD R.T.

7.74 0.49 ug/1 141342 1,4-Dichlorobenzene-d4 11.67

Hit# of 5 Tentative ID MW MolForm CAS# Qual

12-Propanone, /T,1,1-trichloro- 160 C3H3C13O 000918-00-3 39 2 2-Pentanet ol 104 C5H12S 002084-19-7 9 3 4-Penten-2 -one 84 C5H80 013891-87-7 9 4 Acetic acid, dichloro-, ethyl ester 156 C4H6C12O2 000535-15-9 9 Abundance Scan 294 (7.740 min): 29783.D (-) m/ z 4 2.95 100.00% 43

5000 t—i—r । । । । । । । i-t । । । । , . । 7.40 7.601 7.80 8.00 50 56 63 70 83 97 103 119 127 m/z-> 10 20 30 2440 50 * 1 | Tt 1 |*I‘I ' | • » • • | 14 | । । T— TTTTT i Cl i [ 1 60 70 80 90 100 110 120 130 m/ Z 4 .05 10.45% Abundance #12247: 2-Propanone, 1,1,1-trichloro- 43

5000 7,40 7.60 7.80 8.00 m/ z 126.80 8.22% 15 35 ,49 85 97 117 125 'i • ■ ■ ' । ■••■।■ ■ ■ ■ । • m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #1933: 2-Pentanethiol 43 61 7.40 7.60 7.80 8.00 27 55 5000 71 104 m/z 124.95 7.92%

35 —....... ............. - miz-> Abundance 10 20 30 40 43 50 60 70 80 #555: 4-Penten-2-one 90 100 110 120 130

7.40 7.60 A 7.80 8.00 m/z 96.85 7.38%

5000

15

m/z—> ........_ 37 ' ' I ' ' ' ' I ' 10 20 — 371 30 50 53 60 69 4070 i ■ ■ । ■ ■ ■ ■ । « « 1 1 । 80 84 90 100 110 120 130 ■ i ■ i > > i ■ ■ > ■ i . ■ • > i ■ • > • । ■ i ■ 7.40 7.60 7.80 8.00

29783.D GCMS1126.M Fri Dec 28 13:15:34 2001 Page 5

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