GCMS analysis results for sample AD29783, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC1401\29783.D Vial: 6 Acq On : 15 Dec 2001 7:25 am Operator: 209 GALOS Sample : gems scan 12/10 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library . : C:\DATABASE\NBS75K.L ********************************************************★* *********** Peak Number 6 Butanamide Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

8.63 34.97 ug/1 10146600 1,4-Dichlorobenzene-d4 11.67

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Butanamide 87 C4H9NO 000541-35-5 64 2 2-Hexanone, 3-hydroxy-3,5-dimethyl- 144 C8H1602 006321-14-8 39 3 2-Pentanol, 2-methyl- 102 C6H140 000590-36-3 38 4 2-Propanol, 2-methyl- 74 C4H10O 000075-65-0 36 Abundance Scan 391 (8.630 min): 29783.D (-) m/z 59.05 100.00% 59

5000 43

69 80 87 95 .. 151 8.20 8.40 8.60 8.80 9.00

mlz-> 0 -36 107 123 136 ii 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 TIT ।। . ■ ■ ■ । i ' ■ ■ m/z 43.00 35.76% Abundance #62880: Butanamide 44 59

5000 —m — 8.20 8.40 3.60 8.80 9.00 27 72 m/ z 4! . 00 15.85% 87 ■ । ■ • ■ ■ । • ■ ■ • । • ' I' '' ' I ' ■ ' . l' m/z—> 20 30 40 50 60 80 90 100 110 120 130 140 150 160 70 Abundance #8436: 2-Hexanone, 3-hydroxy-3,5-dimethyl- 59

8.20 8.40 8.60 8.80 9.00 5000- m/z 150.90 7.05% 43 101 IL 69 83 111 1i '' 1 1 1 1 1 ''i ' 1 1111 11 'I 1 1 1 1 I 11'1 I' 1 1 1 1 1 1' 1I ' 1 1' i ''' ■ i■■ '■ i ■■■ ■ i■ ■■'i ■■ ■'i'■ m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #63532: 2-Pentanol, 2-methyl- ------------ —4 59 8.20 8.40 8.60 8.80 9.00 m/z 152.90 6.81% 5000- 45 87 31 69 . i TTT.................. ।।।।। . 11111111111 'I' 11 ' i ' m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 8.20 8.40 8.60 8.80 9.00

29783.D GCMS1126.M Fri Dec 28 13:15:41 2001 Page 6

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