GCMS calibration data sheet, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC3101\LBA.D Vial: 5 Acq On : 31 Dec 2001 2:51 pm Operator: 209 GALOS Sample : gems scan 12/14 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 1-Butanamine, 3-methyl- Concentration Rank. 1

R.T. EstConc Area Relative to ISTD R.T.

7.61 4.50 ug/1 888430 1,4-Dichlorobenzene-d4 11.67

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1-Butanamine, 3 -methyl - 87 C5H13N 000107-85-7 9 2 Silane, tetramethyl- 88 C4H12Si 000075-76-3 9 3 Pentane, 3-methoxy- 102 C6H140 036839-67-5 9 4 Butane,/2-methoxy-2-methyl-_______ 102 C6H140 000994-05-8 9 Abundance / Scan 280 (7.614 mln): LBA.D (-) m/z 73.00 1 00.00% 73

5000 43 i ■ ■ ' ' i 1 rl ' I ' 1 1 1 I ' • i • • 103 7.20 7.40 7.60 7.80 8.00 38 , 50 55, . 67, i ,' ■ ‘ i ' ' 87 ' 1 i ■ ■ ‘ ‘ i ' i ' m/z 43.00 32.73% miz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #763: 1-Butanamine, 3-methyl- 30

5000 I ‘ 1 ‘ 1 i ‘ ‘ ' i • ■ ‘ ' I ' ''H 1 1 7.20 7.40 7.60 7.80 8.00 m/z 45.05 12.23% 15 i 41 55 70 87 । । । ‘ ।11 I । • i • 11 ' i ■ ■ ■ ■ I ■ ■ ■ • i ■ ■ ■'■ i ‘ ■ 1 1 I 1 1 1 1 I 1 m/z-> 10 • ■ । 1 । 20 ■ 30 40 50 60 70 80 90 100 110 Abundance #62932; Silane, tetramethyl- 73 *“* | . . r > | i ■ TTTT 7.20 7.40 7.60 7.80 8.00 5000 m/ z 41.05 11.87% 45 15 53 59 88 ‘ ■ i ■ ■ • ■ i 1 ■ ' • i ■ ‘ ■ ■ i ■ ■ ■ ■ i ‘ m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #1793: Pentane, 3-methoxy- —FTPITTTY 73 7.20 7.40 7.60 7.80 8.00 m/z 71.00 7.04% 5000 45

• ■ । 27 33 39 55 ■1 i ■ • • 1 i ■ ■ 1 'r111 • i1 • •’• i • • • < r' miz-> 10 20 30 40 50 60 70 80 90 100 110 7.20 7.40 7.60 7.808.00

LBA.D GCMS1126.M Wed Jan 16 08:29:21 2002 Page 1

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