GCMS calibration data sheet, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC3101 \LBA.D Vial: 5 Acq On : 31 Dec 2001 2:51 pm Operator: 209 GALOS Sample : gems scan 12/14 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ****** * * ************************************************************* Peak Number 2 Heptadecane Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

23.37 0.42 ug/1 106541 Phenanthrene-dl0 24.98

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Heptadecane 240 C17H36 000629-78-7 (97 2 Eicosane 282 C20H42 000112-95-8 91 3 Pentadecane 212 C15H32 000629-62-9 86 4 Heptadecane, 8-methyl- 254 C18H38 013287-23-5 86 Abundance Scan 1996 (23.368 mln): LBA.D (-) m/z 57.0.0 100.00% 57 43 71 5000 85

99 . rtfinf , । —AmTers 1 113 127 140 240 23.00 23.20 23.40 23.60 i —r —7—— ----**mIPIPTTTT m/z 43.05 73.57% miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #71191: Heptadecane 43 57 71 ! 5000 TTTTTTfTTTTT 85 23.00 23.20 23.40 __ 23.60 m/z 71.10 56.03% 99 113 127 141 240 11 J TT-1E—t1—tt31111111*1/1’’1——-2 —rrmhttrr • ■ i1 ■ ■ ■ i ‘•■i■ • ■ 'i • m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #72323: Eicosane 43 57 Ppi ■ 23.20 * 23.00 mmmPpr pp 23.40 23.60 71 5000- m/ z 85.05 38.44% 85

11 . . i 99 113 127 141 282 H" • 1 ‘ * I ‘ ‘ ‘ • i ‘ miz-> ‘ 40 ' ‘ 60 ' 80 100 120 140’160 180 200 220 240 260 280 Abundance #70274: Pentadecane LA 43 57 23.00 23.20 23.40 23.60 m/z 41.05 33.70% 71 5000 85

rrl ‘ TTs .. ■ r.. 28 113 127 ................... . .... . —MPrMaR miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 23.00 23.20 23.40 23.60

LBA.D GCMS1126.M Wed Jan 16 08:29:26 2002 Page 2

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