GC/MS analysis results, sample AE09770, May 15 2002

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Library Search Compound Report Data File : C:\HPCHEM\l\DATA\MAY1002\9770.D Vial: 12 Acq On : 10 May 2002 11:47 pm Operator: Sample : GC/MS SCAN 5/9 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0510.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Eicosane Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

25.22 0.93 ug/1 97622 Phenanthrene-dl0 25.55

Hit# of 5 Tentative ID MW MolForm CAS# Q 1 Eicosane 282 C20H42 000112-95-8 87 2 Heptadecane 240 C17H36 000629-78-7 83 3 Hexadecane 226 C16H34 000544-76-3 74 4 Docosane 310 C22H46 000629-97-0 72 Abundance Scan 2202 (25.221 min): 9770.D (-) m/z 57.10 100.00% 43 57 71 5000 85 R£ 47 - * 0 192 24.80 25.00 25.20 25.40 25.60

mlz—> _20—40l „ 99 113 127 141 155 . । "i . 1. if 11 rn , I’’’" i ■ ■11 ■1 60 । । 80 100 120 140 160 180 200 220 240 260 280 m/ Z 43.10 75.87% Abundance #72323: Eicosane 43 57

71 5000 85 24.80 25.00 25.20 25.40 25.60 m/ Z 71.20 63.29% .. — 99 113 127 141 ' ■ i . .............. . । । ।।। . 282 mz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #71191: Heptadecane 43 57 3...4 L - A . 71 24,80 25.00 25.20 25.40 25.60 5000 m/z 41.05 38.90% 85

— +"T 99al , TTUmuOT 113127141 240 ———umm—VO9]uCmPTor m/z—> Abundance 20 40 60 80 43 57 100 120 140 160 180 200 220 240 260 280 #70787: Hexadecane —) WA 24.80 25.00 25.20 25.40 25.60 m/ Z 85.15 36.18% 71 5000 85

27 99 113127 141 155 226 j ■ ■ ■ • । ■ 1 — MAA ' 14 .4 m/z—> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 24.80 25.00 25.20 25.40 25.60

9770.D GCMS0510.M Mon May 13 12:10:24 2002 Page 2

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