GCMS analysis results for sample AD31630, Feb 28 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\FEB2102\31630.D Vial: 43 Acq On : 23 Feb 2002 8:31 am Operator: Sample : gc/ms scan 2/21 fb Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title 209 625/TCLP calibration table Library C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Eicosane Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

24.03 0.27 ug/1 32715 Phenanthrene-dl0 25.74

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Eicosane / 282 C20H42 000112-95-8 86 .2 Heptadecane / 240 C17H36 000629-78-7 78 3 Tetradecane 198 C14H30 000629-59-4 72 4 Hexadecane 226 C16H34 000544-76-3 64 Abundance Scan 2068 (24.031 min): 31630.D (-) m/ z 57.00 100.00% 43 57 71

5000- 85

‘"T LV . I ' ' 11 i 99 113......... 23.80 24.00 24.20 24.40

m/z- I ■ ■ ' ■ it I 1 il m/z 43.05 83.26% 20 40 60 80 100 120 140 160-180 200 220 240 260 280 Abundance #72324: Eicosane 43 57

71 / 5000 T ii H - । - 85 23.80 24.00 24.20 24.40 m/ Z 71.00 66.02% 99 I i l 11 1 1 I ' ' ' 1 1 1 1 — l 113 141 155 169 183 197 254 282 m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #71191: Heptadecane 43 57 ■ i ■ ■ 71 23.80 24.00 24.20 24:40 5000 m/z 8 5.05 47.60% i 85

... ..................................... . m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #69661: Tetradecane ■ ■ i ■ • •f' 1 ''i ■ 1 43 57 23.80 24.00 24.20 24.40 m/z 41.0.5 39.41% 71 5000 85

27 . I I — . 99 113 155 198 m/z-> I ' ' ' ' I ' ' 20 40 60 1- -8011 1 100 120 140 160 180 200 220 240 260 280 A ■ 1 i ' 1 ' ' ' ' ■ ' I ' ' ■ ' I ' ' 23.80 24.00 24.20 24.40

31630 .D GCMS0208.M Wed Feb 27 12:08:36 2002 Page 2 NYC-WTC_000038242