GCMS analysis results for sample AE08951, May 2002

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Data File C:\HPCHEM\l\DATA\MAY0602\8951.D Vial: 8 Acq On 6 May 2002 11:10 pm Operator: Sample GC/MS SCAN 4/24 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Eicosane Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

23.88 0.43 ug/1 40835 Phenanthrene-dl0 25.58

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Eicosane 282 C20H42 000112-95-8 90 2 Heptadecane 240 C17H36 000629-78-7 90 3 Hexadecane 226 C16H34 000544-76-3 86. 4 Tetradecane 198 C14H30 000629-59-4 86/ Abundance Scan 2056 (23.883 min): 8951 .D (-) m/ z 57.10 100.00% 57 43 71

5000 85 An m l /1 I l n pP, n 99 113 23.60 23.80 24.00 24.20 ll- i 1 ' III I m/z43.10 72.98% m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #72324: Eicosane 43 57

71 5000 85 23.60 23.80 24.00 24.20 m/z 71.10 67.73% 99 ... j 113 141 155169 183197 t r । iiii [ । । । । । । r r । । । h i |”1 i i r । । । i i । । i i i । i 254 i i i । i । 282 1111m m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #71191: Heptadecane 43 57

71 ... Y . 23.60 23.80 24.00 24.20 m/z 85.15 40.81% 5000 85

4— 99 113127141 "f ~ ~ - । 1 i । f r । । 'i ।'। । । । —। । ~r । i । । । । । । i >' _।'i- 240 । j-1 । । । j i i n । T

m/z—> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #70787: Hexadecane 43 57 23.60 23.80 24.00 24.20 m/z 41.10 36.57% 71 5000 85

27 —H 99 113 127 141 155 226 r ' ' ' r'1 m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 23.60 23.80 24.00 24.20

8951 .D GCMS0501.M Wed May 08 11:51:40 2002 Page 2

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