GC/MS analysis results, sample AE09770, May 15 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\MAY1002\9770.D Vial: 12 Acq On : 10 May 2002 11:47 pm Operator: Sample : GC/MS SCAN 5/9 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0510.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Eicosane Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

26.51 0.86 ug/1 90351 Phenanthrene-dl0 25.55

Hit# Of 5 Tentative ID MW MolForm CAS#

1 Eicosane 282 C20H42 000112-95-81 91 2 Heptadecane 240 C17H36 000629-78-7 91 3 Pentadecane 212 C15H32 000629-62-9 91 4 Tricosane 324 C23H48 000638-67-5 90 Abundance Scan 2343 (26.513 min): 9770.D (-) m/z 57.10 100.00% 57 43 71 5000 85

26.20 26.40 26.60 26.80 —ll —11774 m/z 43.10 75.56% miz-> Abundance 40 60 80 100 120 140 160 180 200 #72323: Eicosane 220 240 260 280 A 43 57 71 5000 85 26.20 26.40 26.60 26.80 m/ Z 71.20 62.72% J T—3BII 199 113 127 141............. 282 m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #71191: Heptadecane 57 43 AA===A-======4 71 26.20 26.40 26.60 26.80 5000 m/z 85.15 40.21% 85

113 127 14199 | ill 240 ■ ■ i ■ ■ ■ 11 ■ ■ TIT TIB i ' ' 1 1 i 1 ' ' 1 i ■ ■ ■ ■ i ' ■ ■ ■ i 1 ■ ' 1 i ' ■ ■ ' i ■ ■ ■ ' i ■ ' ' ' i ' ■ m/z->_____ 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #26001: Pentadecane A ,A,A,4N.Yynnq 4111/ 57 26.20 26.40 26.60 26.80 43 71 m/ z 41.05 34.01%

5000 85

99

m/z-> ■ > l' ■ 40 । ■ ■ 60 +— #.113,127 .... 168.... 212,....... ....... 80 100 120 140 160 180 200 220 240 260 280 ■ ■ i ■ ■ 1 ■ i 26.20 26.40 26.60 26.80 TI

9770.D GCMS0510.M Mon May 13 12:10:25 2002 Page 3

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