GCMS sample analysis report, Feb 2002

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Library Search Compound Report

Data File : C: \HPCHEM\ 1 \DATA\JAN1 80231550.D Vial: 16 Acq On : 19 Jan 2002 6:13 am Operator: 209 GALOS Sample : gc/ms scan 12/31 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 Eicosane Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

28.22 0.38 ug/1 106592 Phenanthrene-dl0 24.77

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Eicosane 282 C20H42 000112-95-8 91 2 Pentacosane 352 C25H52 000629-99-2 91 3 Hexadecane 226 C16H34 000544-76-3 90 4.Pentadecane 212 C15H32 000629-62-9 90 Abundance” Scan 2525 (28.222 min): 31550.D (-) m/z 56.95 100.00% 57 43 71

5000 85 ~) ------ 99 27.80 28.00 28.20 28.40 28.60 | L J 113 127 141 155 169 + 'i । ITt FIT1411,41s‘l4**,*1‘‘I‘’ m/z 43.05 79.41% m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #72326: Eicosane 57 43 i 71 5000 85 27.80 28.00 28.20 28.40 28.60 m/z 71.05 69.44%

m/z-> -rl . 4080 113 127 141 155 .......... 60 1 100 120 140 160 80 200 220 240 260 282 280 Abundance one 3 ket lacosune 43 57 i 27.80 28.00 28.20 28.40 28.60 71 5000 85 m/z 41.05 45.42%

1 113 127 141 155 169 183 197 211 225 m/z-> 40 60 80 100 120 140 160 180 200 220 240 .260 280 Abundance #70788: Hexadecane T T Tor 43 57 27.80 28.00 28.20 28.40 28.60 m/z 85.05 45.15% 71 5000 85

miz-> | , 99 1 13 127 141 155 169 183 TImntTTmpmummemuumamuumOmTm 226 40 60 80 100 120 140 160 180 200 220 240 260 280 j ‘ 1 * * i ‘ Aper 27.80 28.00 28.20 28.40 28.60

31550.D GCMS0103.M Wed Feb 06 15:41:16 2002 Page 5

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