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GCMS analysis results for sample AE10517, May 2002

Machine-extracted title · confidence 100%

GCMS analytical report for sample AE10517 showing unknown compounds and surrogate recovery data from May 21, 2002.

NYC-WTC_000045331–000045343

Folder label: “GCMS X 5/2/02 A 5/12/02

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\MAY1002\10517.D Vial: 40 Acq On : 12 May 2002 4:06 am Operator: Sample : gc/ms scan 5/2 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0510.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Eicosane Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T. 25.21 0.76 ug/1 92020 Phenanthrene-dl0 25.55 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Eicosane 282 C20H42 000112-95-8 87 2 Heptadecane 240 C17H36 000629-78-7 87 3 Octacosane 394 C28H58 000630-02-4 86 4 Hexadecane 226 C16H34 000544-76-3 80 Abundance Scan 2201 (25,210 min): 10517.D (-) m/z 57.10 100.00% 57

5000 85 4 —YTTApMu I ApA M 177 , 113 192 24.80 25.00 25.20 25.40 25.60 i . I . I 11 " ' " '' 'i1' । > ।' 11 >" 11111111111 111111 "i11 r '111111■i111111111111111 1 1 ' 1 1 I m/z 43.05 81.35% m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #72323: Eicosane 57

5000 TUI " । 1 1 1 1 I 1 1 1 1 i 1 ' 85 24.80 25.00 25.20 25.40 25.60 m/z 71.10 62.12%

rn/z-> 40 4U 113 141 I i ! [l i i |" m 1‘ । ।।। । i i । i i i i । i i i i । i i i i । i i i । । iti i । । i r 282 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 i।i । i i j i i। r jn-rr Ti i । i i

Abundance #71191: Heptadecane 57 . P____ A _ AAl W ..P I ' ' 1 ■ I '1’r ' ' | ■ r । . j r'. > TTf 24.80 25.00 25,20 25.40 25.60 5000 m/z 85.15 40.18% 85

141 . 113 240 — ■1111 । > । । । । । । । । । r । i । । i । i i i ' । i > > i । i t i i । i i । । i । । । j i i rf ri i i । i i i i । i i m

m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #74211: Octacosane A 00 43 24.80 25.00 25.20 25.40 25.60 m/ z 41.10 34.32% 71 5000

m/z—> T-rp- 40 12127155 183 211 1,111’0’11’0117111111111111133101007117’11 i1 " ' i ■'1' I " ‘11" " 111111 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 364 1111' A vo W ~ 24.80 25.00 25.20 25.40 25,60

10517.D GCMS0510.M Thu May 16 15:10:30 2002 Page 3

NYC-WTC_000045340

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