GCMS analysis results for sample AE10517, May 2002

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Data File : C:\HPCHEM\l\DATA\MAY1002\10517.D Vial: 40 Acq On : 12 May 2002 4:06 am Operator: Sample : gc/ms scan 5/2 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0510.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 2 Heptadecane Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T. 23.85 0.98 ug/1 118416 Phenanthrene-dl0 25.55 Hit 5 Tentative ID MW MolForm CAS# Qual

(1 Heptadecane — 240 C17H36 000629-78-7 93 2 Hexadecane 226 C16H34 000544-76-3 90 3 Pentadecane 212 C15H32 000629-62-9 90 4 Tridecane, 7-propyl-______________ 226 C16H34 055045-09-5 86 Abundance Scan 2053 (23.853 min): 10517.D (-) m/z 57.10 100.00% 43 57 71 5000 85 1r 1 r V... ' 1 ' 1 1 1 1 1 1 99 . 23.60 23.80 24.00 24.20 —— ll „ j 113 127 140 154 I 1 ' 1—1——mman——C/DB/———0—n——mDTTTTTETT 240 m/z 43.05 82.02% m/z-> 40 I60 80 100 120 140 160 180 200 220 240 Abundance #71194: Heptadecane 43 57

71 5000 J V i ■ 1 ■ • i 1 1 i 1 ■ 85 23.60 23.80 24.00 24.20 m/z 71.10 66.93% | 98 113 127 141 155 169 183 212 240 ■ 1 r' 1 1 1 i 1 1 1 I | 1 I I Tj 1 I T l I 1 I I | I I 11 l r I I | TTI I j ! I I-1 | I I I I l T m/z-> 40 60 80 100 120 140 160- 180 200 220 240 Abundance #70789: Hexadecane 43 57

23.60 23.80 24.00 24.20 5000 71 m/ Z 85.15 38.59% 85

,■ ,■ .Ii ■ ,1 ,' 1 i,i ,' ,1 il +1 , 89 113127 .. ..... 226 m/z->______ 40 60 80 100 120 140 160 180 200 220 240 Abundance #70274: Pentadecane ' 1i■■'1।11■ ' i 11 11 । 1 1 57 23.60 23.80 24.00 24.20 43 m/z 41.05 37.55% 71 5000 85

, 99 113 127 141 168 212 1 ■ | l । Q t i । i [ rm t i pm i i j [ i r i i ] i—i—i—t—j—।—।—i—।—[—1—i—i—I—|—i—r m/z—> 40 60 80 100 120 140 160 180 200 220 240 23,60 23.80 24.00 24.20

10517.D GCMS0510.M Thu May 16 15:10:29 2002 Page 2

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