GCMS analysis results for sample AE01462, Feb 2002

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Data File : C:\HPCHEM\l\DATA\FEB2102\1462.D Vial: 15 Acq On : 22 Feb 2002 3:53 am Operator: Sample : gc/ms scan 1/22 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 5 Pentadecane Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

24.03 1.04 ug/1 129090 Phenanthrene-dl0 25.74

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Pentadecane 212 C15H32 000629-62- 9 91 2 Nonadecane 268 C19H40 000629-92-5 91 3 Heptadecane 240 C17H36 000629-78-7 91 / 4 Tricosane 324 C23H48 000638-67-5 91/ Abundance Scan 2068 (24.031 min): 1462.D (-) | m/z 57.00 100.00%; 57 43 71 5000 85

1 TEndI। । I TTT 23.80 24.00 24.20 24.40 — II 4, L ■ i 113 127 141 155 169 ................. . m/z 43.05 73.35% miz-? 40 I60 80 100 120 140 160 180 200 220 240 260 Abundance #26001: Pentadecane 57 43 71 5000 85 . U TTTTrT TT TTTnr 23.80 24.00 24.20 24.40 99 m/ Z 71.00 62.22% — 113 127 212 1 — T 168 • ■ r■ ■ > ■ । > m/z—> 40 60 80 100 120 140 160 180 200 220 240 260 Abundance 57 43 71 - T‘"E 23.80 24.00 24.20 24.40 85 5000 m/z 85.05 44.37%

" 113 127 183 197 268 m/z->... 40 . 60 .. 80__ 100 120 140. 160 180 200 220 240 260 Abundance #71 191: Heptadecane A / 7 T P IPPT 43 23.80 24.00 24.20 24.40 m/z 41.05 36.56% 71 5000 85

il 99 113 127 141 240 ' ’ I ’ ' ’ 1 I I ' T 1 'I ' ‘ f ' l ' ' 1 ' I ' 1 ................... Tu............... ... । . . . I [ > > | | | 7—r — 00 fr AT T f m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 23.80 24.00 24.20 24.40

1462.D GCMS0308.M Mon Mar 25 08:27:34 2002 Page 5

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