GCMS analysis results for sample AE11309, May 28, 2002

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Data File : C:\HPCHEM\1\DATA\MAY2102\11308.D Vial: 22 Acq On : 21 May 2002 9:28 pm Operator: Sample : EXTRACTS/14 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0520.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L Peak Number 4 Pentadecane Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 20.89 0.80 ug/1 64188 Acenaphthene-diO 21.08 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Pentadecane 212 C15H32 000629-62-9 /95 2 Heptadecane 240 C17H36 000629-78-7/91 3 Eicosane 282 C20H42 000112-95-8 91/ 4 Tridecane, 7-propyl- 226 C16H34 _____ 055045-09-5 88 Abundance Scan 1730 (20.892 min): 11308.D (-) m/z 57.10 100. ooi 43 57

71 5000 85 RDn1——PTpT 99 113126 140 212 20.60 20.80 21.00 21.20 l , III ' 4l ' TB —"O—BORBBT—O—OPP)TTmTTTT rn/z43.15 85.47% m/z—>40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #26001: Pentadecane 57 43 71 5000 85 20.60 20.80 21.00 21.20 m/z 71.20 53.77%

m/z-> 40 ■ ■ । > 99 4 40 d 113 127 ........ 168.......... 212 ..................... h 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #71191: Heptadecane 57 43 10 AI—Ar 71 20.60 20.80 21.00 21.20 5000 m/z 41.05 42.62% 85

m/z-> ‘ I‘ 40 ■p-r 60 80 + 99 113 127 141 240 ''I‘' r'i''''i'1''I''''i''''i'■' 1 i ' ' ' ' i ' 1 ' ' 1 1 ' 1 ' I ' 100 120 140 160 180 200 220 240 260 280 Abundance #72323: Eicosane 43 57 20.60 20.80 21.00 21.20 m/ Z 85.15 31.49%I 71 5000 85

m/z—> 1 ' 1 1 40 J60TBB, 80 89 113 127 141 282 AA i j i i ri pi i-1 t । i r

100 120 140 160 180 200 220 240 260 280 20.60 20.80 21.00 21.20

11308.D GCMS0520.M Wed May 22 09:21:19 2002 Page 4

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