GCMS calibration table and instrument parameters, Apr 2002

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Instrument calibration records and method parameters for GCMS analysis of polycyclic aromatic hydrocarbons.

NYC-WTC_000048583–000048597

Folder label: “GCMS X 4/10/02 A 4/15/02”

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NYC 9/11 Public Portal Document

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Data File C:\HPCHEM\1\DATA\APR1202\8481.D Vial: 26 Acq On 16 Apr 2002 9:08 am Operator: Sample gc/ms scan 4/10 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 7 Pentacosane Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T. 15.17 0.30 ug/1 59279 Naphthalene-d8 15.87 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Pentacosane 352 C25H52 000629-99-2 59 2 Tetradecane 198 C14H30 000629-59-4 59 3 Docosane 310 C22H46 000629-97-0 59 4 Eicosane 282 C20H42 000112-95-8 59 Abundance Scan 1103 (15.169 min): 8481 D (-) m/ z 43.05 100.00% 43 57 71

5000 85 AWAL 14.80 15.00 15'20 15.40 . I 4 99 lI ... 127 II.......................... m/ Z 57.00 99.17% '

M ।11111 | I ! > I | ii I I | । i r i । i i | i |“r i “ i “i |“ । “r' r i | i>ii|iiii|iii>|rrii|ii m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #73718: Pentacosane 43 57

71 5000 I I II I I I I I I I [ ! 'I I I I I I 1 I I I 85 14.80 15.00 15.20 15.40 m/z 70.95 fl A 68.94% 99 — 113127141 155169183197211225 /z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance

5000 43 57

71 #69661: Tetradecane

.,Q) A JW . 1 I ' ' 1 1 I ' ' ' ' I ' ' ' 1 1 1 1 1 1 1 1 14.80 15.00 15.20 15.40 m/z 41.05 58.73% 85

27 a,., p,, 99 113 ANA AN 155 198 i ■'1 11 ‘ 1 TT 1 I 1 ' |J 1 1r ■' ■ r 1 ' 1 i 1 1 '1 i 1 1 ' 1 i 1 '' ' i ‘ ' 1' i1 ' '11 1 1 111’111 । 1 1 /z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #72997: Docosane ’ ■ IB’ ′′′′′′ ittr I I , f 1 I I 43 57 14.80 15.00 15.20 15.40 m/z 85.05 41.13% 71 5000 85

i ■ ■ ■ • i" ■ -T 9911 ’’113127 155169183197211 292 310 AAAAA _A ’I’’’’I’’’’I’S’II’’’SIII’ IS’ISIISIIISSIIII I | l"! I 'I 1-10/13 I 1 mfe-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 14.80 15.00 15.20 15.40

8481.D GCMS0412.M Wed Apr 17 09:49:11 2002 Page 7

NYC-WTC_000048594

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Calibration table listing internal standards and response factors for GCMS analysis dated April 16, 2002.

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