GCMS calibration table and instrument parameters, Apr 2002

Machine-extracted title · confidence 90%

Instrument calibration records and method parameters for GCMS analysis of polycyclic aromatic hydrocarbons.

NYC-WTC_000048583–000048597

Folder label: “GCMS X 4/10/02 A 4/15/02”

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NYC 9/11 Public Portal Document

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Data File : C:\HPCHEM\1\DATA\APR1202\8481.D Vial: 26 Acq On : 16 Apr 2002 9:08 am Operator: Sample : gc/ms scan 4/10 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 6 Undecane, 5-methyl- Concentration Rank 8 R.T. EstConc Area Relative to ISTD R.T. 15.01 0.25 ug/1 49180 Naphthalene-d8 15.87

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Undecane, 5-methyl- 170 C12H26 001632-70-8 43 2 Octane, l,l'-oxybis- 242 C16H340 000629-82-3 38 3 Octane, 4-methyl- 128 C9H20 002216-34-4 37 4 Eicosane 282 C20H42 000112-95-8 37 Abundance/ Scan 1086 (15.013 min): 8481 .D (-) m/z 57.00 100.00% 43 57

N 71 85 5000 112 ' ' ' I 1 1 ' ' I ' ' W ■ ■ i ■ ■ 95 14.60 14.80 15.00 15.20 15.40 1 1 1 1 1 T 1tr 4 ___ 111 ' 1 1 hl__________________________________________ 11111111111 1 1 1’’ ’I/ m/z 43.05 84.69% m/z-> 20 40 60 80 100 120 140 160 180 200 220 Abundance #68258: Undecane, 5-methyl- 43 57

5000 71

85 WML 14.60 14.80 15.00 15.20 15.40 112 m/z 71.00 70.46% 99 126 140 155 170 i ■ ■ ' ■ i‘ 1 'i 1 1 1 i ' I ' ' ' ' I ' 1 ‘ ' I 1 ' ' ' I ' 1 ' ' I ' 1 ' ' I ' 1

M lz-> 20 40 60 80 100 120 140 160 180 200 220 Abundance #71251: Octane, 1,1'-oxybis- 57 71 U I 1 - ’ I l 1 > ' ' I ' 1 1 1 I ’"* —I ~r 14.60 14.80 15.00 15.20 15.40 5000 m/z 41.05 60.11% 84 fl 42 112

m/z-> Abundance । ' 1 1 ■ । 1 1 20 40 60 _II r1 1 1 1 । 1 ' । । । > । 80 100 ■ । 120 ■ ■ ■ ■

#65131: Octane, 4-methyl- 140 143 i ■ ' ' i ' ' ' ' i ‘ 160 180 210 224 ' 1 I ' ' ' 1 i 1 ' 200 220 AAWAMWVW 43 14.60 14.80 15.00 15.20 15.40 m/z 85.05 55.72% 5000

57 71 85 27

m/z-> 4 20 40 III I 1............... 128 r ' 1 i ' ' ' ' 1 1 1 1 1 I ‘ 1 1 ' i 1 ' ■ ■ i 1 ' ' ■ i ' ■ 1 UI । । । > । । > । > । । । 60 80 100 120 140 160 180 200 220 on [1/ V V V wo v /A M TT 14.60 14.80 15.00 15.20 15.40

8481.D GCMS0412.M Wed Apr 17 09:49:10 2002 Page 6

NYC-WTC_000048593

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