NYC-WTC_000047701
Calibration table listing internal standards and response factors for GCMS analysis dated April 16, 2002.
1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗Document / 15 pages
GCMS calibration table and instrument parameters, Apr 2002
Machine-extracted title · confidence 90%Instrument calibration records and method parameters for GCMS analysis of polycyclic aromatic hydrocarbons.
NYC-WTC_000048583–000048597Folder label: “GCMS X 4/10/02 A 4/15/02”
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NYC 9/11 Public Portal Document
Library Search Compound Report Data File : C:\HPCHEM\1\DATA\APR1202\8481.D Vial: 26 Acq On : 16 Apr 2002 9:08 am Operator: Sample : gc/ms scan 4/10 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L
Peak Number 5 Cyclopentasiloxane, decamethyl Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T.
14.83 2.51 ug/1 491423 Naphthalene-d8 15.87
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 G1 2 Noradrenaline,/ tetra-TMS 457 C20H43NO3Si4 000000-00-0 37 3 N-(Trifluoroacetyl)-0,0',0''-tris(t 481 C19H34F3NO4Si3 000000-00-0 32 4 N-(Trifluorac/etyl)-0,0',0"-tris (tri 495 C20H36F3NO4Si3 000000-00-0 28 Abundance Scan 1066 (14.829 min): 8481 .D (-) m/z 73.00 100.00% 73
5000 267 355
.............)V............... | ‘ I : i | i i । । | r T I i | r i i i | i i
45 14.40 14.60 14.80 15.00 15.20 ’ 1 I I 108 133154 1 11 11** i' 1 193.223 Lh 293 293 323 1 111 +‘/TI*rII TTT—T —I—r 1 i ' ' 1 ■ i 1 m/ z 267.00 47.36% m/z-> 50 100 150 200 250 300 350 400 450 Abundance #51266: Cyclopentasiloxane, decamethyl- 73
355 267 J 5000 । 1 ■ 1 1 । ■ i 1 1 14.40 14.60 14.80 15.00 15.20 m/z 355.05 46.93% ....... .................................. 207 । 323 n/z-> 50 100 150 200 250 300 350 400 450 Abundance #57357: Noradrenaline, tetra-TMS 73 ...................... / \................ 14.40 14.60 14.80 15.00 15.20 5000 102 355 m/z 356.05 16.24%
45 | 147 442 1 ‘i /z-> 50 100 150 200 250 300 350 400 450 Abundance #58326: N-(Trifluoroacetyl)-O,O',O"-tris(trimethylsilyl)no i 1 1 1 ' i ■ ' 1Et 117 73 14.40 14.60 14.80 15.00 15.20 m/ z 268.00 12.40%| 355 5000
45 I, 126147 193 265 376 481 .............. A............... | i i i i | ■ । । । । i i i i | l i i ■ । । i
m/z-> 50 100 150 200 250 300 350 400 450 14.40 14.60 14.80 15.00 15.20
8481.D GCMS0412.M Wed Apr 17 09:49:09 2002 Page 5
NYC-WTC_000048592
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