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GCMS analysis results for sample AE08017, April 2002

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Laboratory report documenting GCMS analysis of sample AE08017 conducted on April 24, 2002, including surrogate recovery data.

NYC-WTC_000047715–000047724

Folder label: “GCMS X 4/4/02 A 4/12/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\APR1102\8017.D Vial: 23 Acq On : 12 Apr 2002 12:01 pm Operator: Sample : gc/ms scan 4/4 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 2 Cyclopentasiloxane, decamethyl Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

14.83 0.51 ug/1 83764 Naphthalene-d8 15.87 Hit# of 5 Tentative ID MW MolForm CAS# Qual l Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 2 Phenethylamine, N-methyl-. beta. , 3,4 399 C18H37NO3Si3 010538-85-9 3 N- (Trifluoroacetyl) -N,O,O' ,0' ‘-tetr 553 C22H42F3NO4Si4 000000-00-0 38 4 Noradrenaline, tetra-TMS _________ 457 C20H43NO3Si4 000000-00-0 37 Abundance Scan 1066 (14.829 min): 8017.D (-) m/z 73.00 100.00% 73

5000 267 355 ...................... ,,..................... 45 14.40 14.60 14.80 15.00 15.20 108 154 193 223 323 m/z-> 1, 11501 '! 100 | । | 150 । i i 200 r |‘ i 250 ■ ■ । ■ r 300 350 i 1 । r | 11 1 —d 11 ■ 1 ■ ■ 1 ■ l -■ ■■ > > l I—mmm 400 450 500 550 m/z 267.00 43.09% Abundance #51266: Cyclopentasiloxane, decamethyl- 73

355 267 / \ 5000 1 1,-1 1 I 14.40 14.60 14.80 15.00 15.20 m/z 355.05 40.70% 207 323, TT PIPTT m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #74239: Phenethylamine, N-methyl-.beta.,3,4-tris(trimethyls 73 — 14,40 14.60 14.80 15.00 15.20 5000 355 m/z 356.05 13.49% 44

m/z-> 1 ' 'I ' 1 50 147 193 267294 1‘*In/I/InII/a/nI-n/nnIII —**IIIIIIIIIIIIIIIIII|III 100 150 200 250 300 350 400 450 500 550 Abundance #60162: N-(TrifIuoroacetyl)-N,O,O',O"-tetrakts(trimethylsi 1 ■ i ■ ■ 73 14.40 14.60 14.80 15.00 15.20 m/z 268.00 10.70% 355 5000

45 .■ |1 । .' 11h.. 1 । 1 ' 147 ' 1 'i ' ■ 1 193 1 i 1 ' ■ 267 ■ i ' ' ' ' i ' ' 1 ■ i 1 1 ■ ■ i 1 1 538 ' 1 i ' ' 1 1 i ' 1 ' 1 I ' 1 - m/z—> 50 100 150 200 250 300 350 400 450 500 550 14.40 14.60 14.80 15.00 15.20

8017.D GCMS0412.M Tue Apr 16 12:08:24 2002 Page 2

NYC-WTC_000047723

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NYC-WTC_000047723Source: NYC Law Department, mirrored locally

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