Laboratory report documenting GCMS analysis of sample AE08012 conducted on April 24, 2002, including surrogate recovery data.
NYC-WTC_000047664–000047672Folder label: “GCMS X 4/4/02 A 4/12/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\l\DATA\APR1102\8012.D Vial: 18 Acq On : 12 Apr 2002 7:06 am Operator: Sample : gc/ms scan 4/4 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L
Peak Number 1 Cyclopentasiloxane, decamethyl Concentration Rank 1
R.T. EstConc Area Relative to ISTD R.T.
14.83 0.52 ug/1 83350 Naphthalene-d8 15.87
Hit# Of 5 'entative ID MW MolForm CAS# Qual 1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 7) 2 Phenethylamine, N-methyl-.beta.,3,4 399 C18H37NO3Si3 010538-85-9 3 Noradrenaline, tetra-TMS 457 C20H43NO3Si4 000000-00-0 37 4 N-(Triflyioroacetyl)-0,0',0' 1-tris (t 481 C19H34F3NO4Si3 000000-00-0 37 Abundance Scan 1066 (14.828 min): 8012.D (-) m/z 73.00 100.00% 73
5000 267 355 / 45 14.40 14.60 14.80 15.00 15.20 108 133154 191 223 ,, 323 , i 1111 Thmp l m/z 355.05 45.91% m/z-> 40 60 80 100120140160180200220240260280300320340360380400420440 Abundance #51266: Cyclopentasiloxane, decamethyl- 73
355 267 5000 14.40 14.60 14.80 15.00 15.20 m/ z 267.00 42.06% I 207 323 . r " ■ i" 111"r 1P "' i" " i' ■ * ■ r ■11111111" I I ■r“"i""i"1 ■ i'r "i"'"r "111 *1 ■ i'1 ■111' Hi m/z-> 40 60 80 100120140160180200220240260280300320340360380400420440 Abundance #74239: Phenethylamine, N-methyl-.beta.,3,4-tris(trimethyls 73 ......... ............. | I I I I | ! I I - I | I I I I | I I I I T t— T 14.40 14.60 14.80 15.00 15.20 5000 355 m/ z 356.05 16.74% 44 .... 147 267 294 193 TTT r "1111" i" " i i'' r ’" i " " r "' r' " i m/z-> 40 60 80 100120140160180200220240260280300320340360380400420440 - Abundance #57357: Noradrenaline, tetra-TMS 73 14.40 14.60 14.80 15.00 15.20 m/z 267.90 11.84%
5000 102 355
45 147 442 i" " i ■" ■ r " 11" " I r"■i I" " i" " r1" i"111" " i" " r "1 r " ■ r "Tr " ■ i" '11" " i" " i I ' ■ ■ 1 i r ' r 1 i 1 ' ' ■ i ■ ' m/z—> 40 60 80 100120140160180200220240260280300320340360380400420440 14.40 14.60 14.80 15.00 15.20
8012.D GCMS0412.M Tue Apr 16 12:07:04 2002 Page 1
NYC-WTC_000047671
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NYC-WTC_000047673
Laboratory report documenting GCMS analysis of sample AE08013 conducted on April 24, 2002, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000047725
Laboratory report documenting GCMS analysis of sample AE08018 conducted on April 24, 2002, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000047682
Laboratory report documenting GCMS analysis of sample AE08014 conducted on April 24, 2002, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000048934
GCMS laboratory report for sample AE08687 analyzed on April 26, 2002, by analyst DLV.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000049157
Laboratory report documenting GCMS analysis of sample AE08835 conducted on April 25, 2002, showing detection of unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000049102
Gas chromatography-mass spectrometry analysis results for sample AE08760 including detection of unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000048867
GCMS laboratory report for sample AE05683 analyzed on April 23, 2002, by analyst DLV.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000048857
GCMS laboratory report for sample AE08682 analyzed on April 23, 2002, by analyst DLV.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000039694
Surrogate recovery data for sample AE06426 analyzed by GCMS on April 18, 2002.
1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000039703
Surrogate recovery data for sample AE06428 analyzed by GCMS on April 18, 2002.
1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000060533
DEP laboratory report of GCMS analysis for sample AE06757 conducted on April 18, 2002.
1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000040079
Laboratory report documenting GCMS analysis of environmental sample AE06998 conducted on April 16, 2002.
1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000047639
Department of Environmental Protection GCMS analysis record dated April 4-12, 2002.
Filed in the same folder
NYC-WTC_000047640
Fragmented page from a GCMS record dated April 12, 2002, containing method parameters and sample identifiers.
Filed in the same folder
NYC-WTC_000047643
Laboratory report of a GCMS blank analysis for sample AE08012 conducted on April 17, 2002, showing non-detect levels for various compounds.
Filed in the same folder
NYC-WTC_000047652
Laboratory report of GCMS calibration data for sample AE08012 conducted on April 17, 2002, listing target compounds and concentrations.
Filed in the same folder
NYC-WTC_000047656
Laboratory report of GCMS reference analysis for sample AE08012 conducted on April 17, 2002, showing recovery percentages for target compounds.
Filed in the same folder