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GCMS results for sample AE08933, April 26, 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE08933 conducted on April 26, 2002.

NYC-WTC_000049370–000049379

Folder label: “GCMS X 4/15/02 A 4/24/02

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Scanned page image, NYC-WTC_000049378
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\APR2302\8933.D Vial: 13 Acq On : 24 Apr 2002 2:07 am Operator: Sample : gc/ms scan 4/15 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L Peak Number 2 Cyclopentasiloxane, decamethyl Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

14.81 0.38 ug/1 63724 Naphthalene-d8 15.84

Hit# of 5 'entative ID MW MolForm CAS# Qual

1 Cyclopentasiloxane, decamethyl - 370 C10H3005Si5 000541-02-6 (87 2 Phenethyl. line, N-methyl-.beta. ,3,4 399 C18H37NO3Si3 010538-85-9 38 3 Noradrena , tetra-TMS 457 C20H43NO3Si4 000000-00-0 37 4 Benzeneethanamine, N-[ (pentafluorop 563 C24H34F5NO3Si3 055429-13-5 32 Abundance Scan 1063 (14.805 min): 8933.D (-) m/z 73.00 100.00% 73

5000 267 355 ........ .. 45 14,40 14.60 14.80 15.00 15.20 ■1 ‘ 'l*" ......... 133 154 193 223 1 £5011B—B91B11111—9—31110/171210920119021017011101/7—73;’........... 323,, J.... ’!44’1’*1114441011111437 l‘‘‘‘IAI‘A++1*1* m/z 267.00 39.44% m/z-> 40 60 80 100120140160180200220240260280300320340360380400420440 Abundance #51266: Cyclopentasiloxane, decamethyl- 73

355 267 5000 14.40 14.60 14.80 15.00 15.20 m/z 355.05 38.41% 207 323 , T’A0000*mummgm Bmmmmmauea—nmda"Bm—0230399 mfe-> 40 60 80 100120140160180200220240260280300320340360380400420440 Abundance #74239: Phenethylamine, N-methyl-.beta.,3,4-tris(trimethyIs 73 1 14.40 14.60 14.80 15.00 15.20 5000 355 m/z 356.05 14.41% A 44

miz-> Abundance 4 147 *mOpmgpTm 193 267 294 40 60 80 100120140160180200220240260280300320340360380400420440 #57357: Noradrenaline, tetra-TMS 73 14.40 14.60 14.80 15.00 15.20 m/z 267.90 12.37%

5000 102 355

45 147 442 TTTTTTTpT-rtpnTnYnnvp-rTTp-rTTpT-rTp-rrTp-rTTp-rrTpT-rr^^ i ‘1 ■ ■ i" “ i “ ■ ‘ ‘ I ‘ ‘ ' 1 I ‘ ' m/z—> 40 60 80 100120140160180200220240260280300320340360380400420440 14.40 14.60 14.80 15.00 15.20

8933.D GCMS0412.M Wed Apr 24 08:38:36 2002 Page 2

NYC-WTC_000049378

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NYC-WTC_000049378Source: NYC Law Department, mirrored locally

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