Laboratory report documenting GCMS analysis of sample AE02568 conducted on March 25, 2002, identifying other unknown compounds.
NYC-WTC_000038891–000038900Folder label: “GCMS X 3/4/02 A 3/20/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Library Search Compound Report
Data File : C:\HPCHEM\1\DATA\MAR1902\2568.D Vial: 23 Acq On : 21 Mar 2002 2:42 am Operator: Sample : gc/ms scan 3/4 fb Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library- : C:\DATABASE\NBS75K.L
Peak Number 2 Cyclopentasiloxane, decamethyl Concentration Rank 1
R.T. EstConc Area Relative to ISTD R.T.
14.86 2.03 ug/1 351622 Naphthalene-d8 15.90
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5000541-02-6 83 2 Phenethylamine, N-methyl-.beta. , 3,4 399 C18H37NO3Si3 010538-85-9 47 3 Noradrenaline, tetra-TMS 457 C20H43NO3Si4 000000-00-0 37 4 N-(Trifluoracetyl)-0,OO"-tris(tri 495 C20H36F3NO4Si3 000000-00-0 32 Abundance Scan 1070 (14.865 min): 2568.D (-) m/z 73.00 100.00% 73
267 5000
45 i 355 —...L... - 14.60 14.80 15.00 15.20 96 115133 154 193 223 249 | 323 i " i''" i" ■ ‘ i Tmau TTTT “T । m [ TITT । TT TTTTIT 111 TETTUT I "'•I''"I m/ z 2 67.00 48.72% m/z-2 40 60 80 100120140160180200220 240 260280300320340 360 380400420440 Abundance #51266: Cyclopentasiloxane, decamethyl- 73
355 5000 267 /y 14.60 14.80 15.00 15.20 m/z 355.05 44.44% 207 249 | 323 | TITTT TTUT TUITTT I r—i TTTg TTTTIT ' r "' i" " r""r " 'I"'' i" " i"r 1 r11 m/z~> 40 60 80 100120140160180200220240260280 300320340 360380400420440 Abundance ’■ " aa;i , . . 73
____14.60 14.80 15.00 15.20 5000 355 m/z 356.0,5 16.06% 44 147 193 267 294 m/z->......... 40.. 60.. 80 100120140160180 200 220 240 260 280 300 320 340 360 380 400 420 440 Abundance #57357: Noradrenaline, tetra-TMS 73 14.60 14.80 15.00 15.20 m/z 268.0.0 12.07% 5000 102 355
45 | 147 11011011111 | < । iI.... p I 442 1111J111111111J) 111111IV11111! 111 ■ J ■ 11! J, 111111 f I I I I J I I | | | '1 I , | , I t , | , I m/z-> 40 60 80 100120140160180200220240260280300320340 360380400420440 | 14.60 14.80 15.00 15.20
2568.D GCMS0308.M Thu Mar 21 14:20:57 2002 Page 2
NYC-WTC_000038899
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NYC-WTC_000038901
Laboratory report documenting GCMS analysis of sample AE02567 conducted on March 25, 2002, identifying other unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000038827
Laboratory report documenting GCMS analysis of sample AE02579 conducted on March 25, 2002, identifying other unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000038861
Laboratory report documenting GCMS analysis of sample AE02576 conducted on March 25, 2002, identifying other unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000038817
Gas chromatography-mass spectrometry analysis of sample AE04336 conducted on March 25, 2002, identifying other unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000038074
Laboratory report listing detection results for volatile organic compounds in sample AE03830 analyzed on March 29, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000038064
Laboratory report listing detection results for volatile organic compounds in sample AE03829 analyzed on March 29, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000038054
Laboratory report listing detection results for volatile organic compounds in sample AE03828 analyzed on March 29, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000038773
Laboratory note documenting the re-extraction and re-analysis of sample AE02565 due to low recovery rates.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000040088
Laboratory report documenting GCMS analysis of environmental sample AE06997 conducted on April 16, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000040146
Laboratory report documenting GCMS analysis of sample AE06991 conducted on April 16, 2002, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000011728
Laboratory report documenting GCMS analysis of sample AE04039 conducted on April 1, 2002, by analyst DLV.
1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000046673
Laboratory report documenting GCMS analysis of sample AE07318 conducted on April 10, 2002.
1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000038747
Department of Environmental Protection site log sheet for the World Trade Center area dated March 2002.
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NYC-WTC_000038748
Fragmented page from a DEP laboratory record showing method parameters and sample data for March 2002.
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NYC-WTC_000038752
Laboratory report listing quantitative results for volatile organic compounds in sample AE02567 analyzed on March 21, 2002.
Filed in the same folder
NYC-WTC_000038756
Laboratory report listing quantitative results for volatile organic compounds in sample AE02567 analyzed on March 21, 2002.
Filed in the same folder
NYC-WTC_000038764
Laboratory report showing non-detectable levels of target volatile organic compounds in a GCMS blank sample.
Filed in the same folder