NYC-WTC_000011949
Technical record of GCMS calibration data for TCLP analysis using sample vial 14 from March 28, 2002.
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GCMS calibration table for TCLP analysis, March 2002
Machine-extracted title · confidence 100%Technical record of GCMS calibration data for TCLP analysis using sample vial 13 from March 28, 2002.
NYC-WTC_000011942–000011948Folder label: “GCMS X 2/28/02 A 3/26/02”
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NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\l\DATA\MAR2502\4386.D Vial: 13 Acq On : 25 Mar 2002 10:02 pm Operator: Sample : gc/ms scan 2/28 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Cyclopentasiloxane, decamethyl Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T.
14.84 1.66 ug/1 271369 Naphthalene-d8 15.89
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 68 2 Phenethylamine, N-methyl-.beta.,3,4 399 C18H37NO3Si3 010538-85-9 38 3 Noradrenaline, tetra-TMS 457 C20H43NO3Si4 000000-00-0 37 4 Benzeneethanamine, N- [ (pentafluorop 563 C24H34F5NO3Si3 055429-13-5 37 Abundance Scan 1067 (14.845 min): 4386.D (-) m/z 73.00 100.00% 73
5000 267 355
45 14.60 14.80 15.00 15.20
miz-> n , 108 133 154 TImgTuegor 193 223.249,1..,2 293 323 L .. 40 60 80 100120140160180200220240260280300320340360380400420440 m/z 267.00 43.61% Abundance #51266: Cyclopentasiloxane, decamethyl- 73
355 ...... ) 267 5000 1 rI 1 1 ‘ 1 1 1 1 ■ ■ । ■ 1 1 i 1 1 14.60 14.80 15.00 15.20 m/z 355.0 39.16% .. . ।.. ........ 207.. 249.... ............. m/z—_ 40 60 80 100120140160180 200 220 240 260 280 300 320 340 360 380400 420 440 Abundance - hhyi ;:.■■■■ 1,3 drsimmmi*ls 73 ......... ........
14.60 14.80 15.00 15.20 5000 355 m/z 356.05 14.12% 44 147 193 267 294 "’IE1EE10EIETOETTI"ICDOIUD—BBIB—U-I"“WIIOOOUISICCOWTEOOTETOTTTT mfe-> 40 60 80 100120140160180200220240260280300320340360380400420440 Abundance #57357: Noradrenaline, tetra-TMS 73 14.60 14.80 15.00 15.20 m/z 268.00 10.07% 5000 102 355
45 r —233133011 1’29187018011 147. ..... .. ...!... . m/z~>___ 40 60 80 100 120140160180 200 220 240 260280 300 320 340 360 380400420440 ................. 14.60 14.80 15.00 15.20
4386.D GCMS0308.M Thu Mar 28 12:29:37 2002 Page 1
NYC-WTC_000011947
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