GCMS analysis results for sample AE05683, April 23, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\APR1202\8683.D vial: 15 Acq On : 15 Apr 2002 9:48 pm Operator: Sample : gc/ms scan 4/11 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C: \DATABASE\NBS75K. L ********************************************************************* Peak Number 2 Cyclopentasiloxane, decamethyl Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 14.83 1.37 ug/1 228646 Naphthalene-d8 15.87 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 90 2 Noradrenaline, tetra-TMS 457 C20H43NO3Si4 000000-00-0 37 3 Benzeneethanamine, N-[(pentafluorop 563 C24H34F5NO3Si3 055429-13-5 32 4 N-(Trifluoracetyl)-N,0,0‘,0 ’’-tetr 553 C22H42F3NO4Si4 000000-00-0 28 Abundance Scan 1066 (14.829 min): 8683.D (-) m/z 73.00 100.00% 73 4

5000 267 355

......... l\_____ 45 14.40 14.60 14.80 15.00 15.20 125154 193223 , 323 [ '■ 4* feri 104 11 * J11'. **1.1 m-rt . . OI/** m/z 355.05 49.11% iz-> 50 100 150 200250300350400450500550 Abundance #51266: Cyclopentasiloxane, decamethyl- 73

355 267 — 5000 14.40 14.60 14.80 15.00 15.20 m/z 267.00 46.30%

niz-> 50 100 150 207 200 250 43234 300 350 400 450 500 550 Abundance #57357: Noradrenaline, tetra-TMS 73

14.40 14.60 14.80 15.00 15.20 5000 102 355 m/z 356.05 17.09%

45 I 147 442 1 1 ‘ i ' ■ ■ ■ i ■ ■ ■ ■ i ■ ■

mfe-> 50 100 150 200 250 300 350 400 450 500 550 - Abundance #74706: Benzeneethanamine, N-[(pentafluoropheny!)methylene] 73 355 14.40 14.60 14.80 15.00 15.20 m/z 267.90 13.43% 5000

m/z—> 45 _L TT1a—B—208 1 ' i ■ ■ 50 251 281 U—-TmTT ‘Iu386 100 150 200 250 300 350 400‘450 ‘ 500 550 458 548 L V 14.40 14.60 14.80 15.00 15.20

8683.D GCMS0412.M Tue Apr 16 15:42:46 2002 Page 2

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