GCMS surrogate recovery data, sample AE11573, May 30, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\l\DATA\MAY2102\11573.D Vial: 6 Acq On : 22 May 2002 6:20 am Operator: Sample : EXTRACTS/20 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0520.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Cyclopentasiloxane, decamethyl Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 14.75 0.44 ug/1 33152 Naphthalene-d8 15.78 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 64 2 Benzeneethanamine, N-[ (pentafluorop 475 C21H26F5NO2Si2 055429-85-1 28 3 Noradrenaline, tetra-TMS 457 C20H43NO3Si4 000000-00-0 16 4 Phenethylamine, N-methyl-.beta., 3,4 399 C18H37NO3Si3 010538-85-9 9 Abundance Scan 1060 (14.754 min): 11573.D (-) m/ z 73.10 100.00% 73

5000 267 355 14.40 14.60 14.80 15.00

mfz~> 4—+ 45

50 154 ' I 1 1 1 1 I ' 1 1 1 f' i ' 100 150 193 200 250 • i ■ 300 ■ • 350 • i ■ 1 ■ ■ i 1 ■ ■ ■ 400 1 1 ‘I m/z 267.05 27.488 Abundance #51266: Cyclopentasiloxane, decamethyl- 73

355 267 5000 14.40 14.60 14.80 15.00 m/z 355.00 23.52%

■ ■ i ..................... 207 .32.... m/z—> 50 100 ' ' ‘l50' ‘ ‘ 200 250 300 350 400 Abundance #74573: Benzeneethanamine, N-[(pentafluorophenyI)methylene] 73 14.40 14.60 14.80 15.00 “ ‘ ' 5000 m/z 356.00 7.93% 267 44

miz-> L 50 h,. 100 151 179 209 237 1f*****1* 150 200 250 300 ■ i ■ ■ ‘ ' 350 i ■ 400 T Abundance #57357: Noradrenaline, tetra-TMS 1 ■ । ■11 ‘ i ■ ? ■ ■ i ■ ■1' i11 ■' i ‘ 73 14.40 14.60 14.80 15.00 m/z74.10 7.59 5000 102 355

45

m/z—> TI- 50 47 200 150 250 ..... 300 350 • 1 i ' ■ ‘ 442 ■ i ' ‘ i • ■ • ‘ i • ■ • ■ i • ■ • • i ■ ■ ■ ■ i ' 100 400 14.40 14.60 14.80 15.00

11573.D GCMS0520.M Wed May 22 13:58:22 2002 Page 2

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