GCMS analysis results for sample AE06456, April 2002

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Laboratory report documenting GCMS analysis of sample AE06456 conducted on April 19, 2002, by the DEP.

NYC-WTC_000039611–000039627

Folder label: “GCMS X 3/19/02 A 4/17/02”

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NYC 9/11 Public Portal Document

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Data File : C:\HPCHEM\1\DATA\APR1702\6456.D Vial: 14 Acq On : 17 Apr 2002 8:55 pm Operator: Sample : gc/ms scan 3/19 fb Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Cyclopentasiloxane, decamethyl Concentration Rank 9

R.T. EstConc Area Relative to ISTD R.T.

14.81 0.23 ug/1 32238 Naphthalene-d8 15.85

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6(90 2 N-(Trifluoroadetyl)-N,0,0',0''-tetr 553 C22H42F3NO4Si4 000000-00-0 43 3 Benzeneethanamine, N-[(pentafluorop 563 C24H34F5NO3Si3 055429-13-5 38 4 Noradrenalin tetra-TMS 457 C20H43NO3Si4 000000-00-0 37 Abundance Scan 1064 (14.810 min): 6456. D (-) m/z 73.00 100.00% 73 |

5000 267 355 — I 1 1....... ............. f I I I I I U 1 I I I ] > I TT I I I

45 191 14.40 14.60 14.80 15.00 15.20 L i । 1 ' i 1 1 ■ ' i 1 1 ' ■ i ' ‘ 1 ' i 1 ' 1 ' i ' ' 1 1 i ' m/z 266.90 47.61% m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #51266: Cyclopentasiloxane, decamethyl- 73

355 267 5000 - i 1 ■ ■ ■ i ■ 14.40 14.60 14.80 15.00 15.20 m/z 355.05 42.21% 207 323, ■ 1 i 1 1 1 ■ i ' ' ' ' i 1 ■ • ' 1110 m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #60162: N-(Trifluoroacetyl)-N,O,O',O,'-tetrakis(trimethylsi 73 111 355 14.40 14.60 14.80 15.00 15.20 5000 m/z 356.05 16.46%

45 L 147 193 267 [ 538 ' 1 i 1 1 mz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #74706: Benzeneethanamine, N-[(pentafluorophenyl)methylene] i 1 ' ■ 1 i ■ ■ ■ 1 i 1 ■ 1 1 i 1 1 ■ ■ i ■ ' 73 14.40 14.60 14.80 15.00 15.20 355 m/z 267.90 12.20%

5000

45 208 251 281 386 458 548 ■ 1 । 1 1 ' 1 । 1 ■ 1 1 । ■ TPPfT PT | । 1 ■ 1 |*> ■ m/z—> 50 100 150 200 250 300 350 400 450 500 550 14.40 14.60 14.80 15.00 15.20

6456.D GCMS0412.M Thu Apr 18 09:15:04 2002 Page 2

NYC-WTC_000039619

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NYC-WTC_000039619Source: NYC Law Department, mirrored locally

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GCMS analysis results for sample AE06452, April 2002 · Box DEP Box 23

NYC-WTC_000039545

Laboratory report documenting GCMS analysis of sample AE06452 conducted on April 19, 2002, by the DEP.

1 shared topics · Same agency, volume and box · similarity 0.998