GCMS sample analysis results, AE11597, May 30, 2002

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Laboratory report presenting analytical results for target compounds and surrogate recovery data for water sample AE11597.

NYC-WTC_000012710–000012719

Folder label: “GCMS X 5-20-02 A 5-22-02”

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C: \HPCHEM\ 1 \DATA\MAY2 10211597.D Vial: 11 Acq On : 22 May 2002 1:14 pm Operator: Sample : EXTRACTS/20 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L *** * * **************************************************************** Peak Number 2 Cyclopentasiloxane, decamethyl Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 14.75 0.42 ug/1 33546 Naphthalene-d8 15.78

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 72 2 Benzeneethanamine, N-[ (pentafluorop 563 C24H34F5NO3Si3 055429-13-5 25 3 Noradrenaline, tetra-TMS 457 C20H43NO3Si4 000000-00-0 25 4 Benzeneethanamine, N-[ (pentafluorop 475 C21H26F5NO2Si2 055429-85-1 25 Abundance Scan 1060 (14.754 min): 11597.D (-) m/ z 73.10 100.00% 73

5000 267 355 * * । • • • • । • t ■ ■ • • i»• 1* < j > 45 14.40 14.60 14.80 15.00 — . .... 193 ... i............. m/z 266.95 26.35% mlz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #51266: Cyclopentasiloxane, decamethyl- 73

355 267 5000 14.40 14.60 14.80 15.00 m/z 355.10 26.24% .. ...... 207 _ 323' ............................................ ■ ■ ।■■‘■। * * ‘■।■ ■ • ‘ i' 1 • ■ । ■ miz-> 50 100 150 200 250 360 350 '460 '450 560 550 Abundance #74706: Benzeneethanamine, N-[(pentafluorophenyl)methylene] 73 355 14.40 14.60 14.80 15.00 ‘ ‘ 5000 m/z 356.00 9.47%

45 | I 208 251 281 386 458 548 ■ ■ i ■ ■ ■ ' i • ■ ■ ■ i * • ■ i ■ ——— , 41411.* miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #57357: Noradrenaline, tetra-TMS 73 14.40 14.60 14.80 15.00 ' ‘ ' rn/z 74.10 8.51% 5000 102 355

45 147 1 । 442 • ’ I ‘ ' *1*,+*/+h"*+'I'1 ‘ 1 i ‘ ‘ ‘ i ‘ ‘ ■ i ‘ 1 ■ • i • ■ ■ ' i ■ • ■ ■ i • • • • i • ■ miz—> 50 100 150 200 250 300 350 400 450 500 550 14.40 14.60 14.80 15.00 '

11597.D GCMS0501.M Thu May 23 08:19:48 2002 Page 2

NYC-WTC_000012718

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NYC-WTC_000012718Source: NYC Law Department, mirrored locally

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NYC-WTC_000012673

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