GCMS results for sample AE09676, May 2002

Machine-extracted title · confidence 95%

Laboratory report of GCMS analysis for sample AE09676 conducted on May 23, 2002, showing surrogate recovery data.

NYC-WTC_000023811–000023827

Folder label: “GCMS X 5/9/02 A 5/20/02”

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\l\DATA\MAY0602\9676 .D Vial: 19 Acq On 7 May 2002 9:55 am Operator : Sample GC/MS SCAN 4/25 FB Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: May 9 8:46 2002 Quant Results File: GCMS0501.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table . ,

W Last Update : Wed May 01 10:40:31 2002 Response via : Initial Calibration DataAcq Meth : GCMS0501

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 12.19 152 682824 40.00 ug/1 -0.02 10) Naphthalene-d8 15.83 136 2492011 40.00 ug/1 -0.02 17) Acenaphthene-diO 21.13 164 1363838 40.00 ug/1 -0.02 30) Phenanthrene-diO 25.58 188 1911134 40.00 ug/1 -0.02 38) Chrysene-dl2 33.63 240 1069378 40.00 ug/1 -0.03 44) Perylene-dl2 37.87 264 647102 40.00 ug/1 -0.02

System Monitoring Compounds 28) TCMX 23.27 209 35771 5.39 ug/L -0.02 Spiked Amount 10.000 Recovery = 53.90% Target Compounds Qvalue 2) N-nitroso-dimethyl amine 0.00 74 0 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 12.10 146 203 N.D. 5) 1,4-Dichlorobenzene 12.10 146 203 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2‘-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) Isophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 15.72 180 103 N.D. 15) Naphthalene 15.88 128 575 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. 22) Acenaphthylene 0.00 152 0 N.D. 23) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 0.00 165 0 N.D. 25) Diethylphthalate 22.62 149 476 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 29) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D. 31) N-Nitrosodiphenylamine 0.00 168 0 N.D. 32) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 33) Hexachlorobenzene 0.00 284 0 N.D. 34) Phenanthrene 25.63 178 504 N.D. (#) = qualifier out of range (m) = manual integration 9676.D GCMS0501.M Thu May 09 08:47:30 2002 Page 1

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GCMS instrument log for sample AE10065, May 2002 · Box DEP Box 18

NYC-WTC_000023728

Instrument log and analysis summary for GCMS testing of sample AE10065 conducted on May 23, 2002.

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