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GCMS sample analysis results, AE11599, May 30, 2002

Machine-extracted title · confidence 100%

Laboratory report presenting analytical results for target compounds and surrogate recovery data for water sample AE11599.

NYC-WTC_000012729–000012738

Folder label: “GCMS X 5-20-02 A 5-22-02

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Scanned page image, NYC-WTC_000012737
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\l\DATA\MAY2102\11599.D Vial: 13 Acq On : 22 May 2002 3:12 pm Operator: Sample : EXTRACTS/20 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Cyclopentasiloxane, decamethyl Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

14.75 0.46 ug/1 33117 Naphthalene-d8 15.78 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 2 Benzeneet namine, N-[(pentafluorop 475 C21H26F5NO2Si2 055429-85-1 25 000541-02-6 33 3 Noradrena ine, tetra-TMS 457 C20H43NO3Si4 000000-00-0 25 4 Benzoic a cid,2,6-bis[(trimethylsil370C16H3004Si3 003782-85-2 9 Abundance / Scan 1059 (14.750 min): 11599.D (-) m/z 73.10 100.00% 73 )

5000

267 355 ' ■ i ■ ■ • ■ i ■ ■ • ■ i ■ 1 ■ 1 i ■ ■ ■ ■ i • 14.40 14.60 14.80 15.00 , 154 193 I, mmmmppTpTpg "ITCIOIT m/z 355.10 22.10% m/z-> 40 60 80 100120140160180200220240260280300320340360380400420440 Abundance #51266: Cyclopentasiloxane, decamethyl- 73

355 267 5000 1440 14.60 14.80 15.00 ' ‘1' m/z 266.95 21.45% 207 —"“ ।.... ।.... 323 , ‘ [ TTTTT1*002""— ।।.... ।.... ।.... ।11111 mz-> 40 60 80 100120140160180200220240260280300320340360380400420440 Abundance #74573: Benzeneethanamine, N-[(pentafluorophenyl)methylene] 73 14.40 14.60 14.80 15.00 5000 m/z 356.10 9.05% 267 44 ... 151 179 299 237 TMUmmppm mz-> 40 60 80 100120140160180200220240260280300320340360380400420440 Abundance #57357: Noradrenaline, tetra-TMS i ' ' ■ 1 i 1T 73 14.40 14.60 14.80 15.00 m/z 74.10 8.30% 5000 102 355

45 147 442 Tmmpn I....|....|....1|.,u]. i,, | p-rTTjTTTTyrrrrp-rrT-j- 1 T IT m/z—> 40 60 80 100120140160180200220240260280300320340360380400420440 14.40 14.60 14.80 15.00

11599.D GCMS0501.M Thu May 23 08:20:11 2002 Page 2

NYC-WTC_000012737

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NYC-WTC_000012737Source: NYC Law Department, mirrored locally

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