GCMS analysis page, sample AE04848, March 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\MAR2602\4848 .D vial: 21 Acq On 27 Mar 2002 5:32 am Operator: Sample gc/ms scan 3/7 Inst ; GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Cyclopentasiloxane, decamethyl Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

14.85 1.08 ug/1 264084 Naphthalene-d8 15.88

Hit# of 5 Tohtative ID MW MolForm CAS# Qual

1 Cyclopentas^oxane, decamethyl - 370 C10H3005Si5 000541-02-6 68 2 N-(Trifluo/oacetyl)-N,O,O' ,0''-tetr 553 C22H42F3NO4Si4 000000-00-0 38 3 Benzoic a/id, 2,4-bis[(trimethylsil 370 C16H30O4Si3 010586-16-0 38 4 NoradrenMine, tetra-TMS 7 G2 0H43NO3 Si 4 _.000000-00-0 _____ 37 Abundance t Scan 1068 (14.847 min); 4848.D। m/ z 7(3

5000 267 355

I ‘ ' 45 96 125 154 / 93 223 14.60 14.80 15.00 15.20__ 293 323 . Um m/z 267.00 44.61% 50 100 150 200 250 300 350 400 450 500 550 'Abundance .#51266; Cyclopentasiloxane, decamethyl- 713

355 5000 267 l\...... I ' ' ' ' I ' ‘ ‘ I ' ‘ 14.60 14.80 15.00 15.20 m/z 355.05 43.35% I 207 . I 323 ;m/z->50 100 150 200 250 300 350 400 450 500 550 Abundance #<’0162: N-ttnfiijcroacGtyij-N 0.6 .O"-{etrakis(trirne!hylsi 73

355 14.60 14.80 15.00 15.20 5000 m/z 356.05 15.52%

45 I I 147 193 267 ................... 538 , 50 100 150 200 250 300 350 400 450 500 550 Abundance #73975: Benzoic acid, 2,4-bis[(trimethylsilyljoxy]-, trimet T 73 14.60 14.80 15.00 15.20 m/z 268.00 12.10% 5000 355 45

'm/z-> 133 -193 223 rT-T-ii-T-i-i-rT-TM-r-r-r-i-j-^-A-r-T-i-r 50 100 150 200 250 281 300 350 400 450 500 550 l\ . 14.60 14.80 15.00 15.20

4848.D GCMS0308.M Fri Mar 29 11:34:18 2002 Page 1

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