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GCMS sample analysis results for AE01964, March 2002

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Laboratory report detailing the analytical results for sample AE01964 obtained via GCMS on March 22, 2002.

NYC-WTC_000010332–000010341

Folder label: “GCMS X 1/27/02 A 2/26/02 - 3/5/02 3/20/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\MAR1902\1964.D Vial: 10 Acq On : 20 Mar 2002 7:59 am Operator: Sample : gc/ms scan 3/5 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Cyclopentasiloxane, decamethyl Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

14.86 0.26 ug/1 52653 Naphthalene-d8 15.90

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 50 2 N-(Trifluoroacetyl)-N,0,0',0 ''-tetr 553 C22H42F3NO4Si4 000000-00-0 43 3 Noradrenaline/ tetra-TMS 457 C20H43NO3Si4 000000-00-0 37 4_3,4-Dihydroxybenzyl alcohol,tris(tr 356 C16H3203Si3 068595-79-9 37 Abundance Scan 1070 (14.864 min): 1964.D (-) m/z 73.00 1 00.00% 73

5000 267 355 k 14.60 14.80 15.00 15.20 45 154 193 223 , — Pr m/z 267.00 42.12% m/z->. ..50 100. 150 200 250 300 350 400 450 500 550 Abundance #51266: Cyclopentasiloxane, decamethyl- 73

355 267 5000 II 1 ■ * i f * * * i * • 14.60 14.80 15.00 15.20 m/z 355.05 40.71% 207 323 m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance 73

355 14.60 14.80 15.00 15.20 5000 m/z 356.05 16.40%

45 147 193 267 538 ■ ' I ' ' ' 1 I ‘ m/z-> 50 100 150 2dO 250 300 350 400 450 ' 500 ' 550 Abundance #57357: Noradrenaline, tetra-TMS 73 14.60 14.80 15.00 15.20 m/z 268.00 11.16% 5000 102 355

45 I 147 k......... 442 .................. m/z-> 50 100 150 200 250 300 350 400 450 500 550 14.60 14.80 15.00 15.20

1964.D GCMS0308.M Thu Mar 21 09:16:36 2002 Page 1

NYC-WTC_000010339

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NYC-WTC_000010339Source: NYC Law Department, mirrored locally

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